2,4-Pyrimidinediamine, 6-(1-methylethyl)-5-(4-nitrophenyl)-

Base Information

Chemical Name:2,4-Pyrimidinediamine, 6-(1-methylethyl)-5-(4-nitrophenyl)-
CAS No.:634199-49-8
Molecular Formula:C13H15N5O2
Molecular Weight:273.294
Hs Code.:
DSSTox Substance ID:DTXSID70473828
Wikidata:Q82303467

Synonyms:634199-49-8;6-ISOPROPYL-5-(4-NITROPHENYL)PYRIMIDINE-2,4-DIAMINE;2,4-Pyrimidinediamine, 6-(1-methylethyl)-5-(4-nitrophenyl)-;DTXSID70473828

Suppliers and Price of 2,4-Pyrimidinediamine, 6-(1-methylethyl)-5-(4-nitrophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-Pyrimidinediamine, 6-(1-methylethyl)-5-(4-nitrophenyl)-

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:273.12257474
Heavy Atom Count:20
Complexity:338

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C1=C(C(=NC(=N1)N)N)C2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of 2,4-Pyrimidinediamine, 6-(1-methylethyl)-5-(4-nitrophenyl)-

There total 6 articles about 2,4-Pyrimidinediamine, 6-(1-methylethyl)-5-(4-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 34062-03-8
6-isopropyl-5-phenyl-pyrimidine-2,4-diamine

: 634199-49-8
6-isopropyl-5-(4'-nitrophenyl)-pyrimidine-2,4-diamine

Guidance literature:: With sulfuric acid; nitric acid; at 0 - 20 ℃; for 2h;
DOI:10.1081/SCC-120024725

Reference yield:

: 4-methyl-2-(4-nitro-phenyl)-3-oxo-pentanenitrile

: 113-00-8
guanidine nitrate

: 634199-49-8
6-isopropyl-5-(4'-nitrophenyl)-pyrimidine-2,4-diamine

Guidance literature:: 4-methyl-2-(4-nitro-phenyl)-3-oxo-pentanenitrile; With diazomethyl-trimethyl-silane; In dichloromethane; at 20 ℃;

guanidine nitrate; In ethanol; Heating;
DOI:10.1016/j.bmcl.2006.01.012

Reference yield:

: 555-21-5,34512-13-5,174848-08-9
4-Nitrophenylacetonitrile

: 634199-49-8
6-isopropyl-5-(4'-nitrophenyl)-pyrimidine-2,4-diamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; DMAP / CH₂Cl₂ / 20 °C

2.1: TMSCHN₂ / CH₂Cl₂ / 20 °C

2.2: ethanol / Heating

With dmap; triethylamine; diazomethyl-trimethyl-silane; In dichloromethane;
DOI:10.1016/j.bmcl.2006.01.012