5'-Adenylic acid, monophenyl ester

Base Information

Chemical Name:5'-Adenylic acid, monophenyl ester
CAS No.:63554-93-8
Molecular Formula:C16H18N5O7P
Molecular Weight:423.322
Hs Code.:

Synonyms:

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Chemical Property of 5'-Adenylic acid, monophenyl ester

Chemical Property:

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Technology Process of 5'-Adenylic acid, monophenyl ester

There total 3 articles about 5'-Adenylic acid, monophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 58-61-7
adenosine

: 681035-22-3
(2-oxo-5,5-diphenyl-oxazolidin-3-yl)-phosphonic acid diphenyl ester

: 63554-93-8
[5']adenylic acid monophenyl ester

Guidance literature:: adenosine; (2-oxo-5,5-diphenyl-oxazolidin-3-yl)-phosphonic acid diphenyl ester; With N,N'-bis(benzyliden)ethylendiamine; copper(II) bis(trifluoromethanesulfonate); triethylamine; In dichloromethane; at 20 ℃; for 48h;

With water; silica gel; In methanol;
DOI:10.1021/ol051104n

Reference yield:

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 63554-93-8
[5']adenylic acid monophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 74 percent / n-BuLi / hexane; tetrahydrofuran / 2 h / 20 °C

2.1: copper(II) triflate; N,N'-ethylenebis(benzaldimine); Et₃N / CH₂Cl₂ / 48 h / 20 °C

2.2: 49 percent / silica gel; H₂O / methanol

With n-butyllithium; N,N'-bis(benzyliden)ethylendiamine; copper(II) bis(trifluoromethanesulfonate); triethylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol051104n

Reference yield:

: 63554-93-8
[5']adenylic acid monophenyl ester

Guidance literature:: aus 6-Benzamido-9-β-D-ribofuranosylpurin-5'-phenylhydrogenphosphat und 1n NaOCH3 in sd.Me. <70 Min.> Ausb.:88percent;
DOI:10.1021/ja00869a023