Silane, trimethyl[3-phenyl-1-[(trimethylsilyl)oxy]-1-propenyl]-

Base Information

Chemical Name:Silane, trimethyl[3-phenyl-1-[(trimethylsilyl)oxy]-1-propenyl]-
CAS No.:63578-13-2
Molecular Formula:C15H26OSi2
Molecular Weight:278.53700
Hs Code.:

Synonyms:3-phenyl-1-trimethylsiloxy-1-trimethylsilylpropene;1-trimethylsiloxy-1-tri methylsilyl-3-phenyl-1-propene;

Suppliers and Price of Silane, trimethyl[3-phenyl-1-[(trimethylsilyl)oxy]-1-propenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Silane, trimethyl[3-phenyl-1-[(trimethylsilyl)oxy]-1-propenyl]-

Chemical Property:

PSA：9.23000
LogP:4.84190

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of Silane, trimethyl[3-phenyl-1-[(trimethylsilyl)oxy]-1-propenyl]-

There total 6 articles about Silane, trimethyl[3-phenyl-1-[(trimethylsilyl)oxy]-1-propenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 77078-51-4
S-methyl 3-phenylpropanethioate

: 77078-54-7
3-phenylthiopropionic acid

: 63578-13-2
1-(trimethylsilyl)-3-phenyl-1-(trimethylsiloxy)-1-propene

Guidance literature:: With sodium; In benzene; for 4.5h; Ambient temperature;
DOI:10.1246/bcsj.53.2634

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 61157-31-1
3-phenylpropionyltrimethylsilane

: 63578-13-2
1-(trimethylsilyl)-3-phenyl-1-(trimethylsiloxy)-1-propene

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 20 min, 2.) a) -78 deg C, 5 min, b) 25 deg C, 5 min;
DOI:10.1021/ja00170a026

Reference yield:

: 645-45-4
hydrocinnamic acid chloride

: 63578-13-2
1-(trimethylsilyl)-3-phenyl-1-(trimethylsiloxy)-1-propene

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Et₃N / toluene / 17 h / Heating

2: 1.) lithium diisopropylamide (LDA) / 1.) THF, -78 deg C, 1 h, 2.) r.t., 2 h

3: 1.) Na / 1.) benzene, 0 deg C to r.t., 2.) benzene, reflux, 2 h

With sodium; triethylamine; lithium diisopropyl amide; In toluene;
DOI:10.1016/S0040-4020(01)90375-8