2-[(4-chlorobenzoyl)oxy]-1H-isoindole-1,3(2H)-dione

Base Information

Chemical Name:2-[(4-chlorobenzoyl)oxy]-1H-isoindole-1,3(2H)-dione
CAS No.:63591-89-9
Molecular Formula:C15H8ClNO4
Molecular Weight:301.686
Hs Code.:
DSSTox Substance ID:DTXSID70490813
Nikkaji Number:J3.156.249J
Wikidata:Q82334829

Synonyms:63591-89-9;2-[(4-chlorobenzoyl)oxy]-1H-isoindole-1,3(2H)-dione;1,3-dioxoisoindolin-2-yl 4-chlorobenzoate;SCHEMBL11073957;1H-Isoindole-1,3(2H)-dione, 2-[(4-chlorobenzoyl)oxy]-;DTXSID70490813;ZIBXHQBHUBKJGH-UHFFFAOYSA-N;EN300-6513734;1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl 4-chlorobenzoate

Suppliers and Price of 2-[(4-chlorobenzoyl)oxy]-1H-isoindole-1,3(2H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-[(4-chlorobenzoyl)oxy]-1H-isoindole-1,3(2H)-dione

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:301.0141854
Heavy Atom Count:21
Complexity:435

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(=O)N(C2=O)OC(=O)C3=CC=C(C=C3)Cl

Technology Process of 2-[(4-chlorobenzoyl)oxy]-1H-isoindole-1,3(2H)-dione

There total 8 articles about 2-[(4-chlorobenzoyl)oxy]-1H-isoindole-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 524-38-9
N-hydroxyphthalimide

: 104-88-1
4-chlorobenzaldehyde

: 63591-89-9
1,3-dioxoisoindolin-2-yl 4-chlorobenzoate

Guidance literature:: With tert.-butylnitrite; In acetonitrile; at 80 ℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1021/acs.orglett.1c03434

Reference yield: 95.0%

: 524-38-9
N-hydroxyphthalimide

: 74-11-3
para-chlorobenzoic acid

: 63591-89-9
1,3-dioxoisoindolin-2-yl 4-chlorobenzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; at 20 ℃; for 2h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.7b01950

Reference yield: 92.0%

: 524-38-9
N-hydroxyphthalimide

: 873-76-7
para-Chlorobenzyl alcohol

: 63591-89-9
1,3-dioxoisoindolin-2-yl 4-chlorobenzoate

Guidance literature:: With tert.-butylhydroperoxide; oxygen; In acetonitrile; at 20 ℃; for 18h; Reagent/catalyst; Solvent; Catalytic behavior; Irradiation; Sealed tube;
DOI:10.1002/asia.201900878