1-Methyl-8-phenyl-1H-purine-2,6(3H,7H)-dione

Base Information

Chemical Name:1-Methyl-8-phenyl-1H-purine-2,6(3H,7H)-dione
CAS No.:2850-37-5
Molecular Formula:C12H10 N4 O2
Molecular Weight:242.237
Hs Code.:2933990090
Mol file:2850-37-5.mol

Synonyms:1H-Purine-2,6-dione,3,7-dihydro-1-methyl-8-phenyl- (9CI); Xanthine, 1-methyl-8-phenyl- (7CI,8CI);1-Methyl-8-phenylxanthine; 8-Phenyl-1-methylxanthine; NSC 282736

Suppliers and Price of 1-Methyl-8-phenyl-1H-purine-2,6(3H,7H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 1-Methyl-8-phenyl-1H-purine-2,6(3H,7H)-dione

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：83.54000
Density:1.398g/cm³
LogP:0.61690

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Methyl-8-phenyl-1H-purine-2,6(3H,7H)-dione

There total 12 articles about 1-Methyl-8-phenyl-1H-purine-2,6(3H,7H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5770-20-7
6-benzylamino-1-methyl-5-nitrosopyrimidine-2,4(1H,3H)-dione

: 2850-37-5
8-Phenyl-1-methylxanthine

Guidance literature:: In xylene; for 2.5h; Heating;
DOI:10.1021/jm00126a014

Reference yield: 50.0%

: 42963-38-2
6-methyl-<1,2,5>oxadiazolo<3,4-d>pyrimidine-5,7(4H,6H)-dione 1-oxide

: 100-46-9
benzylamine

: 2850-37-5
1-methyl-8-phenylxanthine

Guidance literature:: In N,N,N,N,N,N-hexamethylphosphoric triamide; at 170 ℃; for 5h;

Reference yield:

: 2565-47-1
1-methyl-2,4,6-pyrimidinetrione

: 2850-37-5
8-Phenyl-1-methylxanthine

Guidance literature:: Multi-step reaction with 4 steps

1: 33 percent / POCl₃ / H₂O / 1 h / Heating

2: 52 percent / butan-1-ol / 1 h / Heating

3: 89 percent / sodium nitrite, HOAc / H₂O

4: 95 percent / xylene / 2.5 h / Heating

With acetic acid; sodium nitrite; trichlorophosphate; In water; xylene; butan-1-ol;
DOI:10.1021/jm00126a014