Cyclohexanepropanenitrile, b-methyl-

Base Information

• Chemical Name: Cyclohexanepropanenitrile, b-methyl-
• CAS No.: 64198-20-5
• Molecular Formula: C10H17N
• Molecular Weight: 151.252
• Mol file: 64198-20-5.mol

Synonyms:

Chemical Property of Cyclohexanepropanenitrile, b-methyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanepropanenitrile, b-methyl-

There total 10 articles about Cyclohexanepropanenitrile, b-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

but-2-enenitrile (4786-20-3,627-26-9) + Cyclohexyl iodide (626-62-0) → 3-cyclohexylbutyronitrile (64198-20-5)

Guidance literature:

With sodium tetrahydroborate; tributyltin chloride; In ethanol; at 25 ℃; Irradiation;

Reference yield: 78.0%

crotononitrile (4786-20-3,627-26-9) + Cyclohexyl iodide (626-62-0) → 3-cyclohexylbutyronitrile (64198-20-5) + cyclohexanol (108-93-0)

Guidance literature:

With oxygen; nickel diacetate; In methanol; at 65 ℃; for 1h; Product distribution; other reaction time, temperature, reagent;

DOI:10.1021/jo961751f

Reference yield: 40.0%

1-bromocyclohexane (108-85-0) + crotononitrile (4786-20-3,627-26-9) → 3-cyclohexylbutyronitrile (64198-20-5)

Guidance literature:

With borohydride exchange resin; nickel diacetate; In methanol; at 65 ℃; for 1h;

DOI:10.1021/jo961751f

upstream raw materials:

but-2-enenitrile

Cyclohexyl iodide

allytriphenyltin

<<(methylthio)thiocarbonyl>oxy>cyclohexane