n-(2-Bromoethyl)benzenesulfonamide

Base Information

Chemical Name:n-(2-Bromoethyl)benzenesulfonamide
CAS No.:6453-88-9
Molecular Formula:C8H10 Br N O2 S
Molecular Weight:264.143
Hs Code.:
European Community (EC) Number:848-136-7
NSC Number:121997
DSSTox Substance ID:DTXSID30298251
Wikidata:Q82039947

Synonyms:n-(2-bromoethyl)benzenesulfonamide;6453-88-9;NSC121997;SCHEMBL4235505;DTXSID30298251;AKOS009289451;NSC 121997;NSC-121997;CS-0250212;EN300-50114

Suppliers and Price of n-(2-Bromoethyl)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of n-(2-Bromoethyl)benzenesulfonamide

Chemical Property:

Vapor Pressure:2.4E-05mmHg at 25°C
Boiling Point:359.3°C at 760 mmHg
Flash Point:171.1°C
Density:1.556g/cm³
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:262.96156
Heavy Atom Count:13
Complexity:229

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)S(=O)(=O)NCCBr

Technology Process of n-(2-Bromoethyl)benzenesulfonamide

There total 4 articles about n-(2-Bromoethyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 2576-47-8
2-bromoethylamine hydrobromide

: 98-09-9
benzenesulfonyl chloride

: 6453-88-9
N-(2-bromo-ethyl)-benzenesulfonamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 1.5h; Cooling with ice;

Reference yield: 97.0%

: N-(2-bromo-2-(trimethylsilyl)ethyl)benzenesulfonamide

: 6453-88-9
N-(2-bromo-ethyl)-benzenesulfonamide

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1039/c9ob01689a

Reference yield:

: 98-10-2
benzenesulfonamide

: 6453-88-9
N-(2-bromo-ethyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / dichloromethane / 20 h / 25 °C

2: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C

With N-Bromosuccinimide; potassium tert-butylate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c9ob01689a