5-chloro-2-methyl-1-indanone

Base Information

• Chemical Name: 5-chloro-2-methyl-1-indanone
• CAS No.: 64220-40-2
• Molecular Formula: C10H9ClO
• Molecular Weight: 180.634
• Hs Code.: 2914700090

Synonyms:5-Chloro-2-methyl-2,3-dihydro-1H-inden-1-one;5-chloro-2-methyl-1-indanone;5-Chlor-2-methyl-indan-1-on;5-chloro-2-methyl-indan-1-one;

Chemical Property of 5-chloro-2-methyl-1-indanone

Chemical Property:

• PSA: 17.07000
• LogP: 2.71490
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

5-Chloro-2-methyl-2,3-dihydro-1H-inden-1-one 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-chloro-2-methyl-1-indanone

There total 11 articles about 5-chloro-2-methyl-1-indanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 5-chloro-2-methyl-1-oxo-2,3-dihydro-1H-indene-2-carboxylate → 5-chloro-2-methyl-2,3-dihydro-1H-inden-1-one (64220-40-2)

Guidance literature:

With hydrogenchloride; acetic acid; at 80 ℃; for 1h; Microwave irradiation; Sealed tube;

DOI:10.1016/j.ejmech.2021.113243

Reference yield:

2-chloroisobutyryl chloride (13222-26-9) + chlorobenzene (108-90-7) → 5-chloro-2-methyl-2,3-dihydro-1H-inden-1-one (64220-40-2)

Guidance literature:

With aluminium trichloride;

DOI:10.1021/ja01604a041

Reference yield:

chlorobenzene (108-90-7) + 1,1,1-trichloro-2-methyl-2-propanol (57-15-8) → 5-chloro-2-methyl-2,3-dihydro-1H-inden-1-one (64220-40-2)

Guidance literature:

With aluminium trichloride;

DOI:10.1021/ja01604a041

upstream raw materials:

2-bromo-1-(4-chlorophenyl)-2-methylpropan-1-one

2-chloroisobutyryl chloride

chlorobenzene

1,1,1-trichloro-2-methyl-2-propanol

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