Ethyl phenyl(propan-2-yl)phosphinate

Base Information

Chemical Name:Ethyl phenyl(propan-2-yl)phosphinate
CAS No.:53716-14-6
Molecular Formula:C11H17O2P
Molecular Weight:212.2252
Hs Code.:
NSC Number:201761
DSSTox Substance ID:DTXSID00308058
Nikkaji Number:J3.493.404E

Synonyms:53716-14-6;NSC201761;SCHEMBL17032652;DTXSID00308058;Ethyl phenyl(propan-2-yl)phosphinate;NSC-201761

Suppliers and Price of Ethyl phenyl(propan-2-yl)phosphinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Ethyl phenyl(propan-2-yl)phosphinate

Chemical Property:

Vapor Pressure:0.00675mmHg at 25°C
Boiling Point:279.6°Cat760mmHg
Flash Point:136.9°C
Density:1.03g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:212.09661678
Heavy Atom Count:14
Complexity:207

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(C1=CC=CC=C1)C(C)C

Technology Process of Ethyl phenyl(propan-2-yl)phosphinate

There total 4 articles about Ethyl phenyl(propan-2-yl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 75-30-9
2-iodo-propane

: 172487-18-2,2511-09-3
ethyl Phenylphosphinate

: 53716-14-6
isopropyl-phenyl-phosphinic acid ethyl ester

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; for 6h; Heating;
DOI:10.1021/jo062436o

Reference yield:

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 53716-14-6
isopropyl-phenyl-phosphinic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 3 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

2: triethylamine / 0 - 20 °C / Inert atmosphere; Schlenk technique

With triethylamine; In tetrahydrofuran;
DOI:10.1039/c5cc06389b