2,3-Dimethyl-4-trifluoromethanesulfonyloxybenzaldehyde

Base Information

Chemical Name:2,3-Dimethyl-4-trifluoromethanesulfonyloxybenzaldehyde
CAS No.:643093-73-6
Molecular Formula:C10H9F3O4S
Molecular Weight:282.24
Hs Code.:
DSSTox Substance ID:DTXSID90450196
Wikidata:Q82269799

Synonyms:2,3-dimethyl-4-trifluoromethanesulfonyloxybenzaldehyde;643093-73-6;4-formyl-2,3-dimethylphenyl trifluoromethanesulfonate;SCHEMBL4462296;DTXSID90450196

Suppliers and Price of 2,3-Dimethyl-4-trifluoromethanesulfonyloxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-Dimethyl-4-trifluoromethanesulfonyloxybenzaldehyde

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:3
Exact Mass:282.01736442
Heavy Atom Count:18
Complexity:398

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C=CC(=C1C)OS(=O)(=O)C(F)(F)F)C=O

Technology Process of 2,3-Dimethyl-4-trifluoromethanesulfonyloxybenzaldehyde

There total 4 articles about 2,3-Dimethyl-4-trifluoromethanesulfonyloxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 58380-40-8
2,3-Dimethyl-4-hydroxybenzaldehyde

: 643093-73-6
4-formyl-2,3-dimethylphenyl trifluoromethanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 4885-02-3
Dichloromethyl methyl ether

: 526-75-0
2,3-Dimethylphenol

: 1426547-43-4
6-formyl-2,3-dimethylphenyl trifluoromethanesulfonate

: 643093-73-6
4-formyl-2,3-dimethylphenyl trifluoromethanesulfonate

Guidance literature:: 2,3-Dimethylphenol; With aluminum (III) chloride; In dichloromethane; for 0.166667h; Inert atmosphere;

Dichloromethyl methyl ether; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

trifluoromethylsulfonic anhydride; Overall yield = 95%; Overall yield = 1.8 g; Further stages;
DOI:10.1055/s-0033-1340302