1-(4-Chlorobenzene-1-sulfonyl)-3-methylbenzene

Base Information

Chemical Name:1-(4-Chlorobenzene-1-sulfonyl)-3-methylbenzene
CAS No.:64325-30-0
Molecular Formula:C₁₃H₁₁ClO₂S
Molecular Weight:266.748
Hs Code.:
DSSTox Substance ID:DTXSID40495294
Nikkaji Number:J1.218.464F
Wikidata:Q82343295

Synonyms:64325-30-0;1-(4-Chlorobenzene-1-sulfonyl)-3-methylbenzene;DTXSID40495294

Suppliers and Price of 1-(4-Chlorobenzene-1-sulfonyl)-3-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-Chlorobenzene-1-sulfonyl)-3-methylbenzene

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:266.0168285
Heavy Atom Count:17
Complexity:339

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)S(=O)(=O)C2=CC=C(C=C2)Cl

Technology Process of 1-(4-Chlorobenzene-1-sulfonyl)-3-methylbenzene

There total 9 articles about 1-(4-Chlorobenzene-1-sulfonyl)-3-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 68971-88-0
Tributyl-m-tolyl-stannane

: 98-60-2
4-chlorobenzenesulfonyl chloride

: 64325-30-0
4-chlorophenyl 3-methylphenyl sulfone

Guidance literature:: In chlorobenzene; at 131 ℃; for 48h;

Reference yield:

: 446-34-4
2-fluoro-4-methyl-1-nitrobenzene

: 64325-30-0
4-chlorophenyl 3-methylphenyl sulfone

Guidance literature:: Multi-step reaction with 5 steps

1: Na₂CO₃

2: m-chloro-perbenzoic acid / CH₂Cl₂

3: HCl; Sn

4: NaNO₂; HBF₄

5: H₂SO₄; Celite; Cu₂O / H₂O

With copper(I) oxide; hydrogenchloride; tin; tetrafluoroboric acid; Celite; sulfuric acid; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium nitrite; In dichloromethane; water; 5: Pschorr cyclization;
DOI:10.1021/ol027301t

Reference yield:

: 4284-60-0
2-(4-Chloro-benzenesulfonyl)-4-methyl-phenylamine

: 64325-30-0
4-chlorophenyl 3-methylphenyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: NaNO₂; HBF₄

2: H₂SO₄; Celite; Cu₂O / H₂O

With copper(I) oxide; tetrafluoroboric acid; Celite; sulfuric acid; sodium nitrite; In water; 2: Pschorr cyclization;
DOI:10.1021/ol027301t