1-{4-[(2-hydroxyethyl)amino]phenyl}ethanone

Base Information

• Chemical Name: 1-{4-[(2-hydroxyethyl)amino]phenyl}ethanone
• CAS No.: 30858-79-8
• Molecular Formula: C10H13 N O2
• Molecular Weight: 179.2157
• Mol file: 30858-79-8.mol

Synonyms:Acetophenone, 4'-[(2-hydroxyethyl)amino]- (8CI);4-(2-Hydroxyethylamino)acetophenone; NSC 63637

Chemical Property of 1-{4-[(2-hydroxyethyl)amino]phenyl}ethanone

Chemical Property:

• Vapor Pressure: 2.76E-06mmHg at 25°C
• Boiling Point: 374.9°Cat760mmHg
• Flash Point: 180.5°C
• Density: 1.16g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-{4-[(2-hydroxyethyl)amino]phenyl}ethanone

There total 3 articles about 1-{4-[(2-hydroxyethyl)amino]phenyl}ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

4-Iodoacetophenone (13329-40-3) + ethanolamine (141-43-5) → 4'-(2-Hydroxyethylamino)acetophenon (30858-79-8)

Guidance literature:

With aluminum oxide; copper; potassium hydroxide; for 0.5h;

DOI:10.1055/s-0035-1560173

Reference yield: 21.0%

4-morpholinoacetophenone (39910-98-0) → 4'-(2-Hydroxyethylamino)acetophenon (30858-79-8)

Guidance literature:

With Hg(II)-EDTA; water; for 2.5h;

DOI:10.1515/znb-1999-0210

Reference yield:

→ 4'-(2-Hydroxyethylamino)acetophenon (30858-79-8)

Guidance literature:

p-Amino-acetophenon, 2-Bromaethanol, (chromatographische Abtrennung von (28));

DOI:10.1021/jo00820a001

upstream raw materials:

4-morpholinoacetophenone

4-Iodoacetophenone

ethanolamine

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