1H-Inden-1-ol, 2,3-dihydro-1-methyl-

Base Information

• Chemical Name: 1H-Inden-1-ol, 2,3-dihydro-1-methyl-
• CAS No.: 64666-42-8
• Molecular Formula: C10H12O
• Molecular Weight: 148.205

Synonyms:1-methyl-1-indanol;1-Methylindan-1-ol;1-hydroxy-1-methyl-2,3-dihydro-1H-indene;3-Methylindanol;1-Oxy-1-methyl-hydrinden;1-hydroxy 1-methyl indane;1-METHYL-2,3-DIHYDRO-1H-INDEN-1-OL;

Chemical Property of 1H-Inden-1-ol, 2,3-dihydro-1-methyl-

Chemical Property:

• Melting Point: 57 °C
• Boiling Point: 118 °C(Press: 14 Torr)
• PSA: 20.23000
• Density: 1.068 g/cm3
• LogP: 1.84030

Purity/Quality:

98% ^*data from raw suppliers

1-methyl-2,3-dihydro-1H-inden-1-ol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Inden-1-ol, 2,3-dihydro-1-methyl-

There total 9 articles about 1H-Inden-1-ol, 2,3-dihydro-1-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methyllithium (917-54-4) + inden-1-one (83-33-0) → 1-methyl-1-indanol (64666-42-8)

Guidance literature:

With cerium(III) chloride; In tetrahydrofuran; at -78 ℃; for 3h;

DOI:10.1021/jo00301a002

Reference yield: 83.0%

methyl magnesium iodide (917-64-6) + inden-1-one (83-33-0) → 1-methyl-1-indanol (64666-42-8)

Guidance literature:

In diethyl ether; at 0 ℃; for 2h; Inert atmosphere;

DOI:10.1080/00397911.2016.1274032

Reference yield: 83.0%

inden-1-one (83-33-0) + methyl iodide (74-88-4) → 1-methyl-1-indanol (64666-42-8)

Guidance literature:

methyl iodide; With iodine; magnesium; In diethyl ether; at 25 ℃; Reflux;

inden-1-one; In diethyl ether; at 0 ℃;

With ammonium chloride; In diethyl ether; water;

DOI:10.1016/j.tetasy.2008.12.002

upstream raw materials:

methyl magnesium iodide

inden-1-one

methyllithium

methyl iodide

Downstream raw materials:

2-(4-methoxybenzylidene)-2,3-dihydro-1H-inden-1-one

2-(4′′-dimethylaminobenzylidene)indan-1-one

1-Methylinden

1-methylindane

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