[2,5-Bis(trimethylsilyl)phenyl](trimethyl)silane

Base Information

• Chemical Name: [2,5-Bis(trimethylsilyl)phenyl](trimethyl)silane
• CAS No.: 17864-15-2
• Molecular Formula: C15H30 Si3
• Molecular Weight: 294.66
• Hs Code.: 2931900090
• Mol file: 17864-15-2.mol

Synonyms:Silane,1,2,4-benzenetriyltris[trimethyl- (9CI); Silane, as-phenenyltris[trimethyl-(6CI,7CI,8CI); 1,2,4-Tris(trimethylsilyl)benzene

Chemical Property of [2,5-Bis(trimethylsilyl)phenyl](trimethyl)silane

Chemical Property:

• Vapor Pressure: 0.0202mmHg at 25°C
• Boiling Point: 260.1°Cat760mmHg
• Flash Point: 77.5°C
• PSA: 0.00000
• Density: 0.85g/cm³
• LogP: 3.32220

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [2,5-Bis(trimethylsilyl)phenyl](trimethyl)silane

There total 14 articles about [2,5-Bis(trimethylsilyl)phenyl](trimethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

trimethylsilylacetylene (1066-54-2) → benzene-1,2,4-triyltris(trimethylsilane) (17864-15-2) + 1,3,5-tris(trimethylsilyl)benzene (5624-60-2)

Guidance literature:

With sodium; (DMSC)TiCl₂; In benzene-d6; at 80 ℃; for 5h; Further Variations:; Catalysts; Product distribution;

DOI:10.1021/ja990740b

Reference yield: 98.0%

trimethylsilylacetylene (1066-54-2) → benzene-1,2,4-triyltris(trimethylsilane) (17864-15-2)

Guidance literature:

(DMSC)Ti{η⁶-1,2,4-C6H3(SiMe3)3}; In benzene-d6; at 25 ℃; Activation energy;

DOI:10.1021/ja994543o

Reference yield: 88.0%

chloro-trimethyl-silane (75-77-4) + 1,2,4-Trichlorobenzene (120-82-1,63697-18-7) → benzene-1,2,4-triyltris(trimethylsilane) (17864-15-2)

Guidance literature:

With 1,3-dimethyl-2-imidazolidinone; magnesium; copper(l) chloride; lithium chloride; at 55 ℃; for 17h;

DOI:10.1021/jo4000866

upstream raw materials:

trimethylsilylacetylene

chloro-trimethyl-silane

1,2,4-Trichlorobenzene

4-vinylbenzyl chloride

Downstream raw materials:

1,2,4-triiodobenzene