Tungsten,pentacarbonyl[(isocyano-kC)cyclohexane]-, (OC-6-21)- (9CI)

Base Information

Chemical Name:Tungsten,pentacarbonyl[(isocyano-kC)cyclohexane]-, (OC-6-21)- (9CI)
CAS No.:15603-77-7
Molecular Formula:C₁₂H₁₁NO₅W
Molecular Weight:433.073
Hs Code.:

Synonyms:Tungsten,pentacarbonyl(cyclohexyl isocyanide)- (7CI,8CI); Tungsten, pentacarbonyl(isocyanocyclohexane)-,(OC-6-21)-; Cyclohexane, isocyano-, tungsten complex

Suppliers and Price of Tungsten,pentacarbonyl[(isocyano-kC)cyclohexane]-, (OC-6-21)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tungsten,pentacarbonyl[(isocyano-kC)cyclohexane]-, (OC-6-21)- (9CI)

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of Tungsten,pentacarbonyl[(isocyano-kC)cyclohexane]-, (OC-6-21)- (9CI)

There total 4 articles about Tungsten,pentacarbonyl[(isocyano-kC)cyclohexane]-, (OC-6-21)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: pentacarbonyl(diphenylcarben)wolfram

: 538-75-0
dicyclohexyl-carbodiimide

: 15603-77-7
pentacarbonyl(cyclohexyl isocyanide)tungsten

: 16770-34-6
N-(α-phenylbenzylidene)cyclohexylamine

Guidance literature:: In pentane; adding a stoichiometric amt. of dicyclohexylcarbodiimide to a soln. of the W complex (20°C), reacting (3 h); column chromy. (silica gel), eluting the isocyanide complex (pentane), eluting the Schiff base (ether);

Reference yield: 52.0%

: W(CO)5(C(SCH₃)2)

: 108-91-8,157973-60-9
cyclohexylamine

: 15603-77-7
pentacarbonyl(cyclohexyl isocyanide)tungsten

Guidance literature:: In hexane; to soln. of W-complex in hexane ligand was added, soln. was stirred for10 min under N2 at room temp.; mixt. was reduced to dryness, crystd. from hexane at -20°C;
DOI:10.1021/ic50223a044

Reference yield: 43.0%

: 931-53-3
Cyclohexyl isocyanide

: pentacarbonyl{(2E)/(2Z)-1,3-diethoxy-3-phenylpropenylidene}tungsten

: 15603-77-7
pentacarbonyl(cyclohexyl isocyanide)tungsten

: 128822-66-2
pentacarbonyl(1-cyclohexyl-3,5-diethoxy-1,5-dihydro-5-phenyl-2H-pyrrole-2-ylidene)tungsten

Guidance literature:: In Petroleum ether; (N2); added cyclohexylyl isocyanide to soln. of W-complex at 0°C; allowed to stand for 24 h at room temp.; chromy.; evapd. (vac.); dissolved in pentane;