Benzamide, N-methyl-N-2-pyridinyl-

Base Information

Chemical Name:Benzamide, N-methyl-N-2-pyridinyl-
CAS No.:65052-85-9
Molecular Formula:C13H12N2O
Molecular Weight:212.251
Hs Code.:
DSSTox Substance ID:DTXSID20401353
Nikkaji Number:J1.803.437I
Wikidata:Q82204437

Synonyms:Benzamide, N-methyl-N-2-pyridinyl-;65052-85-9;N-methyl-N-pyridin-2-ylbenzamide;2-(n-methylbenzamido)pyridine;SCHEMBL6316045;DTXSID20401353;AKOS009105840;N-METHYL-N-(PYRIDIN-2-YL)BENZAMIDE;EN300-6479804;Z223364402

Suppliers and Price of Benzamide, N-methyl-N-2-pyridinyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Benzamide, N-methyl-N-2-pyridinyl-

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:212.094963011
Heavy Atom Count:16
Complexity:236

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C1=CC=CC=N1)C(=O)C2=CC=CC=C2

Technology Process of Benzamide, N-methyl-N-2-pyridinyl-

There total 9 articles about Benzamide, N-methyl-N-2-pyridinyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 4597-87-9
2-(N-methylamino)pyridine

: 98-88-4
benzoyl chloride

: 65052-85-9
N-(pyridin-2-yl)-N-methylbenzamide

Guidance literature:: With pyridine; at 20 ℃; for 17h;
DOI:10.1016/j.tet.2011.08.085

Reference yield: 86.0%

: 4597-87-9
2-(N-methylamino)pyridine

: 65-85-0,8013-63-6
benzoic acid

: 65052-85-9
N-(pyridin-2-yl)-N-methylbenzamide

Guidance literature:: benzoic acid; With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 ℃; for 0.5h;

With dmap; In dichloromethane; at 20 ℃; for 0.166667h;

2-(N-methylamino)pyridine; With triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1080/00397911.2020.1747631

Reference yield: 79.0%

: 4597-87-9
2-(N-methylamino)pyridine

: 108-86-1,52753-63-6
bromobenzene

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 65052-85-9
N-(pyridin-2-yl)-N-methylbenzamide

Guidance literature:: With dmap; potassium phosphate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 120 ℃; for 0.5h; Microwave irradiation;
DOI:10.1021/jo102151u