Germane, bis[2,4-bis(trifluoromethyl)phenyl]dichloro-

Base Information

Chemical Name:Germane, bis[2,4-bis(trifluoromethyl)phenyl]dichloro-
CAS No.:650583-83-8
Molecular Formula:C₁₆H₆Cl₂F₁₂Ge
Molecular Weight:569.7
Hs Code.:
DSSTox Substance ID:DTXSID30477029
Nikkaji Number:J1.933.260H
Wikidata:Q82309074

Synonyms:Germane, bis[2,4-bis(trifluoromethyl)phenyl]dichloro-;650583-83-8;DTXSID30477029;Bis-(2,4-bis-trifluoromethyl-phenyl),dichloro-germane

Suppliers and Price of Germane, bis[2,4-bis(trifluoromethyl)phenyl]dichloro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Germane, bis[2,4-bis(trifluoromethyl)phenyl]dichloro-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:12
Rotatable Bond Count:2
Exact Mass:569.8866713
Heavy Atom Count:31
Complexity:572

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1C(F)(F)F)C(F)(F)F)[Ge](C2=C(C=C(C=C2)C(F)(F)F)C(F)(F)F)(Cl)Cl

Technology Process of Germane, bis[2,4-bis(trifluoromethyl)phenyl]dichloro-

There total 2 articles about Germane, bis[2,4-bis(trifluoromethyl)phenyl]dichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 136664-85-2
2,4-(CF₃)2C₆H₃Li

: 10038-98-9
germaniumtetrachloride

: 80426-23-9
(2,6-bis(trifluoromethyl)-phenyl)lithium

: 650583-83-8
bis[2,4-bis(trifluoromethyl)phenyl]dichlorogermane

Guidance literature:: In diethyl ether; hexane; byproducts: LiCl; (N2); Schlenk technique or glovebox; soln. of mixt. of Li compd. (2 equiv.) in Et2O was added dropwise to soln. of GeCl4 (1 equiv.) in hexane at-78°C; soln. was warmed to room temp. and stirred for 2 h; filtered; solvents removed (vac.); distd. (0.01 Torr, 80-90°C); elem. anal.;
DOI:10.1039/b302544f

Reference yield:

: 402-31-3
1,3-bis(trifluoromethyl)benzene

: 10038-98-9
germaniumtetrachloride

: bis[2,6-bis(trifluoromethyl)phenyl]dichlorogermane

: 650583-83-8
bis[2,4-bis(trifluoromethyl)phenyl]dichlorogermane

Guidance literature:: 1,3-bis(trifluoromethyl)benzene; With n-butyllithium; In diethyl ether; at -78 ℃;

germaniumtetrachloride; In hexane; at -78 ℃;
DOI:10.1002/hlca.201200389