Silane, (4-bromo-2,6-dichlorophenyl)triethyl-

Base Information

Chemical Name:Silane, (4-bromo-2,6-dichlorophenyl)triethyl-
CAS No.:650598-50-8
Molecular Formula:C12H17BrCl2Si
Molecular Weight:340.162
Hs Code.:
DSSTox Substance ID:DTXSID60463172
Wikidata:Q82287985

Synonyms:Silane, (4-bromo-2,6-dichlorophenyl)triethyl-;650598-50-8;DTXSID60463172;AKOS024264329

Suppliers and Price of Silane, (4-bromo-2,6-dichlorophenyl)triethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Silane, (4-bromo-2,6-dichlorophenyl)triethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:337.96600
Heavy Atom Count:16
Complexity:201

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC[Si](CC)(CC)C1=C(C=C(C=C1Cl)Br)Cl

Technology Process of Silane, (4-bromo-2,6-dichlorophenyl)triethyl-

There total 3 articles about Silane, (4-bromo-2,6-dichlorophenyl)triethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 650598-44-0
(2,6-dichlorophenyl)triethylsilane

: 650598-50-8
(4-bromo-2,6-dichlorophenyl)triethylsilane

Guidance literature:: With bromine; sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -75 ℃; for 0.75h;
DOI:10.1002/ejoc.200300355

Reference yield:

: 994-30-9
triethylsilyl chloride

: 650598-50-8
(4-bromo-2,6-dichlorophenyl)triethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / sec-butyllithium / cyclohexane; tetrahydrofuran / -75 °C

2: 63 percent / sec-butyllithium; bromine / cyclohexane; tetrahydrofuran / 0.75 h / -75 °C

With bromine; sec.-butyllithium; In tetrahydrofuran; cyclohexane;
DOI:10.1002/ejoc.200300355

Reference yield:

: 541-73-1
1,3-Dichlorobenzene

: 650598-50-8
(4-bromo-2,6-dichlorophenyl)triethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / sec-butyllithium / cyclohexane; tetrahydrofuran / -75 °C

2: 63 percent / sec-butyllithium; bromine / cyclohexane; tetrahydrofuran / 0.75 h / -75 °C

With bromine; sec.-butyllithium; In tetrahydrofuran; cyclohexane;
DOI:10.1002/ejoc.200300355