N'-phenylpiperidine-1-carboximidamide

Base Information

Chemical Name:N'-phenylpiperidine-1-carboximidamide
CAS No.:65069-94-5
Molecular Formula:C12H17N3
Molecular Weight:203.287
Hs Code.:
European Community (EC) Number:855-999-3
Nikkaji Number:J1.496.468A

Synonyms:N'-phenylpiperidine-1-carboximidamide;65069-94-5;N-Phenylpiperidine-1-carboxamidine;AKOS008152076;AKOS011647091;AKOS032950755;CS-0264603;EN300-93403;Z1267875532

Suppliers and Price of N'-phenylpiperidine-1-carboximidamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N'-phenylpiperidine-1-carboximidamide

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:203.142247555
Heavy Atom Count:15
Complexity:213

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCN(CC1)C(=NC2=CC=CC=C2)N

Technology Process of N'-phenylpiperidine-1-carboximidamide

There total 7 articles about N'-phenylpiperidine-1-carboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 62-53-3
aniline

: 477482-01-2
C-imidazol-1-yl-C-piperidin-1-yl-methyleneamine

: 65069-94-5
piperidine-1-carbonimidic acid anilide

Guidance literature:: In tetrahydrofuran; for 18h; Heating;
DOI:10.1021/jo0202381

Reference yield: 21.0%

: 1530-87-6
1-piperidinylcarbonnitrile

: 62-53-3
aniline

: 65069-94-5
N-phenylpiperidine-1-carboximidamide

Guidance literature:: aniline; With sodium hydride; In dimethyl sulfoxide; mineral oil; at 0 ℃; for 0.25h; Inert atmosphere;

1-piperidinylcarbonnitrile; In dimethyl sulfoxide; mineral oil; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c9ob01651a

Reference yield:

: 103-85-5
monophenylthiourea

: 65069-94-5
N-phenylpiperidine-1-carboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / methanol / 17 h / Ambient temperature

2: 2.) 10percent aq. NaOH / 1.) t-BuOH, reflux, 24 h, 2.) CH₂Cl₂

With sodium hydroxide; In methanol;
DOI:10.1055/s-1988-27606