1-Phenyl-2,2-dimethyl-3-butyn-1-ol

Base Information

Chemical Name:1-Phenyl-2,2-dimethyl-3-butyn-1-ol
CAS No.:65108-32-9
Molecular Formula:C12H14O
Molecular Weight:174.243
Hs Code.:
DSSTox Substance ID:DTXSID501253530
Nikkaji Number:J880.196G

Synonyms:65108-32-9;DTXSID501253530;1-Phenyl-2,2-dimethyl-3-butyn-1-ol;alpha-(1,1-Dimethyl-2-propyn-1-yl)benzenemethanol

Suppliers and Price of 1-Phenyl-2,2-dimethyl-3-butyn-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Phenyl-2,2-dimethyl-3-butyn-1-ol

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:174.104465066
Heavy Atom Count:13
Complexity:202

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C#C)C(C1=CC=CC=C1)O

Technology Process of 1-Phenyl-2,2-dimethyl-3-butyn-1-ol

There total 5 articles about 1-Phenyl-2,2-dimethyl-3-butyn-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 100-52-7
benzaldehyde

: 6214-32-0
1-bromo-3-methylbuta-1,2-diene

: 65108-32-9
2,2-dimethyl-1-phenyl-3-butyn-1-ol

Guidance literature:: With n-butyllithium; 1.) hexane, THF, -78 deg C, 30 min; -78 deg C - -40 deg C, 30 min, 2.) -78 deg C - room temperature;

Reference yield:

: 6214-31-9
3-bromo-3-methylbut-1-yne

: 100-52-7
benzaldehyde

: 65108-32-9
2,2-dimethyl-1-phenyl-3-butyn-1-ol

: 38517-08-7
4-methyl-1-phenyl-2,3-pentadien-1-ol

Guidance literature:: With tetraethylammonium perchlorate; In N,N-dimethyl-formamide; at 20 ℃; Electrochemical reaction;
DOI:10.1016/S0040-4020(99)01089-3