Cyclopropanol, 1-(4-methoxyphenyl)-, 3,5-dinitrobenzoate

Base Information

• Chemical Name: Cyclopropanol, 1-(4-methoxyphenyl)-, 3,5-dinitrobenzoate
• CAS No.: 65109-90-2
• Molecular Formula: C₁₇H₁₄N₂O₇
• Molecular Weight: 358.307
• Mol file: 65109-90-2.mol

Synonyms:

Chemical Property of Cyclopropanol, 1-(4-methoxyphenyl)-, 3,5-dinitrobenzoate

Chemical Property:

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclopropanol, 1-(4-methoxyphenyl)-, 3,5-dinitrobenzoate

There total 3 articles about Cyclopropanol, 1-(4-methoxyphenyl)-, 3,5-dinitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxyphenyl magnesium bromide (13139-86-1) → 1-(4-methoxyphenyl)cyclopropyl 3,5-dinitrobenzoate (65109-90-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Cp₂Sm / tetrahydrofuran / a) -78 deg C, 15 min, b) RT, 1 h

2: pyridine / Ambient temperature

With pyridine; (η5-C5H5)2Sm; In tetrahydrofuran;

DOI:10.1016/0040-4020(95)01039-4

Reference yield:

1-(4-methoxyphenyl)cyclopropan-1-ol (15973-65-6) + 3,5-dinitrobenoyl chloride (99-33-2) → 1-(4-methoxyphenyl)cyclopropyl 3,5-dinitrobenzoate (65109-90-2)

Guidance literature:

With pyridine; Yield given; Ambient temperature;

DOI:10.1016/0040-4020(95)01039-4

Reference yield:

→ 1-(4-methoxyphenyl)cyclopropyl 3,5-dinitrobenzoate (65109-90-2)

Guidance literature:

Cyclopropanol 2(p-OCH3), 3,5-Dinitrobenzoylchlorid;

DOI:10.1021/ja00465a040

upstream raw materials:

1-(4-methoxyphenyl)cyclopropan-1-ol

3,5-dinitrobenoyl chloride

4-methoxyphenyl magnesium bromide