Formamide, N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]-

Base Information

• Chemical Name: Formamide, N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]-
• CAS No.: 652990-10-8
• Molecular Formula: C32H35N3O4
• Molecular Weight: 525.648

Synonyms:

Chemical Property of Formamide, N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]-

Chemical Property:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Formamide, N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]-

There total 2 articles about Formamide, N-[5-[(1R)-1-hydroxy-2-[[2-[4-[[(2R)-2-hydroxy-2-phenylethyl]amino]phen yl]ethyl]amino]ethyl]-2-(phenylmethoxy)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N-{2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethyl}-(R)-2-tert-butyldimethylsiloxy-2-(3-formamido-4-benzyloxyphenyl)ethylamine → N-{2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethyl}-(R)-2-hydroxy-2-(3-formamido-4-benzyloxyphenyl)ethylamine (652990-10-8)

Guidance literature:

N-{2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethyl}-(R)-2-tert-butyldimethylsiloxy-2-(3-formamido-4-benzyloxyphenyl)ethylamine; With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; for 20h;

With sodium hydroxide; In tetrahydrofuran; water; for 0.05h;

Reference yield: 77.0%

2-bromo-(R)-1-tert-butyldimethylsiloxy-1-(3-formamido-4-benzyloxyphenyl)ethane → N-{2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethyl}-(R)-2-hydroxy-2-(3-formamido-4-benzyloxyphenyl)ethylamine (652990-10-8)

Guidance literature:

2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethylamine; With sodium hydroxide; In Isopropyl acetate; water; for 0.133333h;

2-bromo-(R)-1-tert-butyldimethylsiloxy-1-(3-formamido-4-benzyloxyphenyl)ethane; With potassium carbonate; In ISOPROPYLAMIDE; at 50 - 90 ℃; for 17h;

With cesium fluoride; In methanol; butanone; at 30 - 37 ℃; for 7.5h;

Reference yield: 91.0%

N-{2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethyl}-(R)-2-hydroxy-2-(3-formamido-4-benzyloxyphenyl)ethylamine (652990-10-8) → milveterol (652990-07-3)

Guidance literature:

N-{2-[4-((R)-2-hydroxy-2-phenylethylamino)phenyl]ethyl}-(R)-2-hydroxy-2-(3-formamido-4-benzyloxyphenyl)ethylamine; With darco G-60; In ethanol; at 50 ℃; for 0.333333h;

With hydrogen; palladium 10% on activated carbon; In ethanol; for 10h; under 1551.49 Torr;

Downstream raw materials:

milveterol

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