Phosphine sulfide, (5-methyl-1,3-phenylene)bis[diphenyl-

Base Information

Chemical Name:Phosphine sulfide, (5-methyl-1,3-phenylene)bis[diphenyl-
CAS No.:653000-28-3
Molecular Formula:C31H26P2S2
Molecular Weight:524.627
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphine sulfide, (5-methyl-1,3-phenylene)bis[diphenyl-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Phosphine sulfide, (5-methyl-1,3-phenylene)bis[diphenyl-

There total 1 articles about Phosphine sulfide, (5-methyl-1,3-phenylene)bis[diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1611-92-3
3,5-dibromotoluene

: 829-85-6
diphenylphosphane

: 653000-28-3
3,5-bis(diphenylphosphinothioyl)toluene

Guidance literature:: 3,5-dibromotoluene; diphenylphosphane; With potassium acetate; palladium dichloride; In N,N-dimethyl-formamide; at 130 ℃; for 24h;

With sulfur; In N,N-dimethyl-formamide; at 120 ℃; for 4h;
DOI:10.1016/j.jorganchem.2003.08.023

Reference yield: 89.0%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 653000-28-3
3,5-bis(diphenylphosphinothioyl)toluene

: 653000-30-7
CH₃C₆H₂(PS(C₆H₅)2)2PtCl

Guidance literature:: In acetic acid; (N2); heating a mixt. of ligand, platinum complex in AcOH at 115°C for 24 h; filtration, washing with MeOH, water, ether;
DOI:10.1016/j.jorganchem.2003.08.023

Reference yield: 72.0%

: 10025-98-6
potassium tetrachloropalladate(II)

: 653000-28-3
3,5-bis(diphenylphosphinothioyl)toluene

: 653000-29-4
CH₃C₆H₂(PS(C₆H₅)2)2PdCl

Guidance literature:: In acetic acid; (N2); heating a mixt. of ligand, palladium complex in AcOH at 115°C for 24 h; filtration, washing with MeOH, water, ether;
DOI:10.1016/j.jorganchem.2003.08.023