3,5-DIETHYL-1,2,4-TRIAZOL-4-YLAMINE

Base Information

• Chemical Name: 3,5-DIETHYL-1,2,4-TRIAZOL-4-YLAMINE
• CAS No.: 6285-28-5
• Molecular Formula: C6H12N4
• Molecular Weight: 140.19
• Hs Code.: 2933990090
• Mol file: 6285-28-5.mol

Synonyms:3,5-diethyl-4h-1,2,4-triazol-4-amine;3,5-diethanyl-4-amino-1,2,4-triazole;diethyl-1,2,4-triazol-4-amine;3,5-diethyl-4-amino-1,2,4-triazole;3,5-diethyl-1,2,4-triazole-4-ylamine;4-amino-3,5-diethyl-4H-1,2,4-triazole;4-amino-3,5-diethyl-1,2,4-triazole;

Chemical Property of 3,5-DIETHYL-1,2,4-TRIAZOL-4-YLAMINE

Chemical Property:

• Vapor Pressure: 0.000556mmHg at 25°C
• Boiling Point: 311.6°C at 760 mmHg
• Flash Point: 142.3°C
• PSA: 56.73000
• Density: 1.21g/cm³
• LogP: 0.69790

Purity/Quality:

98%min ^*data from raw suppliers

3,5-diethyl-4H-1,2,4-triazol-4-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-DIETHYL-1,2,4-TRIAZOL-4-YLAMINE

There total 5 articles about 3,5-DIETHYL-1,2,4-TRIAZOL-4-YLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

propionic acid (802294-64-0,79-09-4) → 4-amino-3,5-diethyl-1,2,4-triazole (6285-28-5)

Guidance literature:

With hydrazine hydrate; for 5h; Heating;

DOI:10.1107/S0108270107026339

Reference yield: 52.0%

propiononitrile (107-12-0) → 4-amino-3,5-diethyl-1,2,4-triazole (6285-28-5)

Guidance literature:

With hydrazine hydrate; at 180 ℃; for 20h;

DOI:10.1021/jm00345a021

Reference yield: 25.0%

methyl 2,2-dimethoxypropionate (10076-48-9) → 4-amino-3,5-diethyl-1,2,4-triazole (6285-28-5) + 2,2-dimethoxypropionohydrazide (141763-09-9) + 4-amino-3,5-bis(1,1-dimethoxyethyl)-4H-1,2,4-triazole (141763-08-8)

Guidance literature:

With hydrazine hydrate; 1.) 120 deg C, 2 d, 2.) 160 deg C, 8 h;

upstream raw materials:

N¹,N²-dipropionylhydrazine

propionic acid

propiononitrile

methyl 2,2-dimethoxypropionate

Downstream raw materials:

4-Chloro-N-(3,5-diethyl-[1,2,4]triazol-4-yl)-benzamidine

(N,N',N,N')-N,N'-(2,2'-(butane-1,4-diylbis(oxy))bis(2,1-phenylene))bis(methan-1-yl-1-ylidene)bis(3,5-diethyl-4H-1,2,4-triazol-4-amine)

C₃₀H₄₂N₈O₂

(N,N',N,N')-N,N'-(4,4'-(butane-1,4-diylbis(oxy))bis(4,1-phenylene))bis(methan-1-yl-1-ylidene)bis(3,5-diethyl-4H-1,2,4-triazol-4-amine)

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