Carbamic acid, [(1S)-2-[[1-[(cyclohexylamino)carbonyl]-1-ethylpropyl][(4-methoxyphenyl) methyl]amino]-2-oxo-1-(phenylmethyl)ethyl]-, phenylmethyl ester

Base Information

• Chemical Name: Carbamic acid, [(1S)-2-[[1-[(cyclohexylamino)carbonyl]-1-ethylpropyl][(4-methoxyphenyl) methyl]amino]-2-oxo-1-(phenylmethyl)ethyl]-, phenylmethyl ester
• CAS No.: 655239-31-9
• Molecular Formula: C37H47N3O5
• Molecular Weight: 613.797

Synonyms:

Chemical Property of Carbamic acid, [(1S)-2-[[1-[(cyclohexylamino)carbonyl]-1-ethylpropyl][(4-methoxyphenyl) methyl]amino]-2-oxo-1-(phenylmethyl)ethyl]-, phenylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Carbamic acid, [(1S)-2-[[1-[(cyclohexylamino)carbonyl]-1-ethylpropyl][(4-methoxyphenyl) methyl]amino]-2-oxo-1-(phenylmethyl)ethyl]-, phenylmethyl ester

There total 1 articles about Carbamic acid, [(1S)-2-[[1-[(cyclohexylamino)carbonyl]-1-ethylpropyl][(4-methoxyphenyl) methyl]amino]-2-oxo-1-(phenylmethyl)ethyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.6%

Cyclohexyl isocyanide (931-53-3) + N-Cbz-L-Phe (1161-13-3) + 4-methoxy-benzylamine (2393-23-9) + pentan-3-one (96-22-0) → N-benzyloxycarbonyl-L-phenylalanyl-(N-(4-methoxybenzyl)-α,α-diethyl)glycine cyclohexylamide (655239-31-9)

Guidance literature:

for 504h;

DOI:10.1016/j.tet.2009.09.022

Reference yield: 84.9%

N-benzyloxycarbonyl-L-phenylalanyl-(N-(4-methoxybenzyl)-α,α-diethyl)glycine cyclohexylamide (655239-31-9) → N-benzyloxycarbonyl-L-phenylalanyl-N-(4-methoxybenzyl)-α,α-diethylglycine

Guidance literature:

With trifluoroacetic acid; In acetonitrile; at 20 ℃;

DOI:10.1016/j.tet.2009.09.022

Reference yield: 84.4%

N-benzyloxycarbonyl-L-phenylalanyl-(N-(4-methoxybenzyl)-α,α-diethyl)glycine cyclohexylamide (655239-31-9) → (N-benzyloxycarbonyl-L-phenylalanyl)-α,α-diethylglycine (655239-27-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; Reflux;

DOI:10.1016/j.tet.2009.09.022

upstream raw materials:

Cyclohexyl isocyanide

N-Cbz-L-Phe

4-methoxy-benzylamine

pentan-3-one

Downstream raw materials:

(N-benzyloxycarbonyl-L-phenylalanyl)-α,α-diethylglycine

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