1-(tert-Butylsulfanyl)-4-iodobenzene

Base Information

Chemical Name:1-(tert-Butylsulfanyl)-4-iodobenzene
CAS No.:65688-19-9
Molecular Formula:C10H13IS
Molecular Weight:292.184
Hs Code.:
DSSTox Substance ID:DTXSID20495792
Wikidata:Q82344144

Synonyms:65688-19-9;1-(tert-Butylsulfanyl)-4-iodobenzene;DTXSID20495792;1-(t-butylsulfanyl)-4-iodobenzene

Suppliers and Price of 1-(tert-Butylsulfanyl)-4-iodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-(tert-Butylsulfanyl)-4-iodobenzene

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:291.97827
Heavy Atom Count:12
Complexity:131

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)SC1=CC=C(C=C1)I

Technology Process of 1-(tert-Butylsulfanyl)-4-iodobenzene

There total 5 articles about 1-(tert-Butylsulfanyl)-4-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 16463-18-6
4-[(1,1-dimethylethyl)sulfanyl]benzene-1-amine

: 65688-19-9
1-(tert-butylsulfanyl)-4-iodobenzene

Guidance literature:: With toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In water; acetonitrile; at 10 - 20 ℃; for 3h;

Reference yield: 44.0%

: 352-34-1
4-fluoro-1-iodobenzene

: 29364-29-2
sodium tert-butyl thiolate

: 65688-19-9
1-(tert-butylsulfanyl)-4-iodobenzene

Guidance literature:: In N,N-dimethyl-formamide; at 70 ℃;
DOI:10.1002/anie.200352179

Reference yield:

: 1849-36-1
para-nitrobenzenethiol

: 65688-19-9
1-(tert-butylsulfanyl)-4-iodobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / 2.5 h / 20 °C

2: tin(ll) chloride / methanol / 2.5 h / 20 °C / Reflux

3: toluene-4-sulfonic acid; sodium nitrite; potassium iodide / acetonitrile; water / 3 h / 10 - 20 °C

With aluminum (III) chloride; toluene-4-sulfonic acid; potassium iodide; tin(ll) chloride; sodium nitrite; In methanol; water; acetonitrile;