[(3-Methyl-1,2-phenylene)bis(oxy)]bis(trimethylsilane)

Base Information

• Chemical Name: [(3-Methyl-1,2-phenylene)bis(oxy)]bis(trimethylsilane)
• CAS No.: 65838-68-8
• Molecular Formula: C13H24O2Si2
• Molecular Weight: 268.503
• DSSTox Substance ID: DTXSID00562597
• Wikidata: Q82446831

Synonyms:65838-68-8;[(3-Methyl-1,2-phenylene)bis(oxy)]bis(trimethylsilane);DTXSID00562597;INBPVSVUSZJONB-UHFFFAOYSA-N;3-Methylcatechol, 2TMS derivative;3-Methylcatechol, bis(trimethylsilyl) ether

Chemical Property of [(3-Methyl-1,2-phenylene)bis(oxy)]bis(trimethylsilane)

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 268.13148307
• Heavy Atom Count: 17
• Complexity: 243

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=C(C(=CC=C1)O[Si](C)(C)C)O[Si](C)(C)C

Technology Process of [(3-Methyl-1,2-phenylene)bis(oxy)]bis(trimethylsilane)

There total 2 articles about [(3-Methyl-1,2-phenylene)bis(oxy)]bis(trimethylsilane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

bis(trifluoromethyl)-difluoro-sulfurane (30341-38-9) + 2,2-Bis-trifluoromethyl-2λ4-benzo[1,3,2]dioxathiole (65838-64-4) → trimethylsilyl fluoride (420-56-4) + 1-Methyl-2,3-bis-trimethylsilanyloxy-benzene (65838-68-8)

Guidance literature:

In tetrahydrofuran; 0°C, 5 h in freshly dried THF;

DOI:10.1021/ja00471a062

Reference yield:

N,O-Bis(trimethylsilyl)trifluoroacetamide (25561-30-2) + 3-methylbenzene-1,2-diol (488-17-5) → 1-Methyl-2,3-bis-trimethylsilanyloxy-benzene (65838-68-8)

Guidance literature:

In acetonitrile; for 0.5h; Ambient temperature;

DOI:10.1002/oms.1210181002

Reference yield: 41.0%

bis(trifluoromethyl)-difluoro-sulfurane (30341-38-9) + 1-Methyl-2,3-bis-trimethylsilanyloxy-benzene (65838-68-8) → trimethylsilyl fluoride (420-56-4) + 4-Methyl-2,2-bis-trifluoromethyl-2λ4-benzo[1,3,2]dioxathiole (65838-65-5)

Guidance literature:

In tetrahydrofuran; 0°C, 5 h in freshly dried THF;

DOI:10.1021/ja00471a062

upstream raw materials:

N,O-Bis(trimethylsilyl)trifluoroacetamide

3-methylbenzene-1,2-diol

bis(trifluoromethyl)-difluoro-sulfurane

2,2-Bis-trifluoromethyl-2λ⁴-benzo[1,3,2]dioxathiole

Downstream raw materials:

trimethylsilyl fluoride

4-Methyl-2,2-bis-trifluoromethyl-2λ⁴-benzo[1,3,2]dioxathiole

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