CHF 2363

Base Information

• Chemical Name: CHF 2363
• CAS No.: 98384-62-4
• Molecular Formula: C₁₀H₁₀N₂O₅S
• Molecular Weight: 270.266
• Mol file: 98384-62-4.mol

Synonyms:

Chemical Property of CHF 2363

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of CHF 2363

There total 2 articles about CHF 2363 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanol (64-17-5) + 3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide (66074-00-8) → 3-(benzenesulfonyl)-4-ethoxyfuroxan (98384-62-4)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1002/jhet.5570330220

Reference yield:

→ 3-(benzenesulfonyl)-4-ethoxyfuroxan (98384-62-4)

Guidance literature:

DOI:10.1039/jr9640000904

Reference yield: 95.0%

3-(benzenesulfonyl)-4-ethoxyfuroxan (98384-62-4) + 2-methylmethoxybenzene (578-58-5) → 4-ethoxy-3-[(2-methoxyphenyl)methyl]furoxan

Guidance literature:

With dipotassium peroxodisulfate; In water; acetonitrile; at 70 ℃; for 48h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.joc.1c01950

upstream raw materials:

ethanol

3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

Downstream raw materials:

C₂₁H₂₅NO₄S

Refernces