5-CHLORO-4-(CHLOROMETHYL)-3-(4-METHOXYPHENYL)ISOXAZOLE

Base Information

• Chemical Name: 5-CHLORO-4-(CHLOROMETHYL)-3-(4-METHOXYPHENYL)ISOXAZOLE
• CAS No.: 65927-01-7
• Molecular Formula: C11H8Cl3NO2
• Molecular Weight: 292.54600

Synonyms:5-Chloro-4-dichloromethyl-3-(4-methoxy-phenyl)-isoxazole;3-p-Anisyl-5-chlor-4-dichlormethylisoxazol;

Chemical Property of 5-CHLORO-4-(CHLOROMETHYL)-3-(4-METHOXYPHENYL)ISOXAZOLE

Chemical Property:

• Boiling Point: 431.0±45.0 °C(Predicted)
• PKA: -5.89±0.50(Predicted)
• PSA: 35.26000
• Density: 1.416±0.06 g/cm3(Predicted)
• LogP: 4.47980

Purity/Quality:

99% ^*data from raw suppliers

5-CHLORO-4-(CHLOROMETHYL)-3-(4-METHOXYPHENYL)ISOXAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-CHLORO-4-(CHLOROMETHYL)-3-(4-METHOXYPHENYL)ISOXAZOLE

There total 1 articles about 5-CHLORO-4-(CHLOROMETHYL)-3-(4-METHOXYPHENYL)ISOXAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 3-(4-methoxyphenyl)isoxazol-5(4H)-one (31709-47-4) → 5-chloro-4-dichloromethyl-3-(4-methoxy-phenyl)-isoxazole (65927-01-7)

Guidance literature:

With trichlorophosphate;

Reference yield: 88.0%

5-chloro-4-dichloromethyl-3-(4-methoxy-phenyl)-isoxazole (65927-01-7) + 1-(4-methoxyphenyl)ethanone (100-06-1) → (Z)-3-[5-Methoxy-3-(4-methoxy-phenyl)-isoxazol-4-yl]-1-(4-methoxy-phenyl)-propenone (122773-55-1)

Guidance literature:

With sodium hydroxide; In methanol; for 1h;

Reference yield: 85.0%

5-chloro-4-dichloromethyl-3-(4-methoxy-phenyl)-isoxazole (65927-01-7) + para-bromoacetophenone (99-90-1) → (Z)-1-(4-Bromo-phenyl)-3-[5-methoxy-3-(4-methoxy-phenyl)-isoxazol-4-yl]-propenone (122773-52-8)

Guidance literature:

With sodium hydroxide; In methanol; for 1h;

upstream raw materials:

N,N-dimethyl-formamide

3-(4-methoxyphenyl)isoxazol-5(4H)-one

Downstream raw materials:

(Z)-1-(4-Bromo-phenyl)-3-[5-methoxy-3-(4-methoxy-phenyl)-isoxazol-4-yl]-propenone

N-[1-[5-Chloro-3-(4-methoxy-phenyl)-isoxazol-4-yl]-meth-(Z)-ylidene]-N'-phenyl-hydrazine

N-[1-[5-Chloro-3-(4-methoxy-phenyl)-isoxazol-4-yl]-meth-(Z)-ylidene]-N'-(4-chloro-phenyl)-hydrazine

(Z)-3-[5-Methoxy-3-(4-methoxy-phenyl)-isoxazol-4-yl]-1-(4-nitro-phenyl)-propenone

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