3-(Methylamino)-1-(thiophen-2-YL)prop-2-EN-1-one

Base Information

Chemical Name:3-(Methylamino)-1-(thiophen-2-YL)prop-2-EN-1-one
CAS No.:663603-70-1
Molecular Formula:C8H9NOS
Molecular Weight:167.232
Hs Code.:
DSSTox Substance ID:DTXSID00697651
Mol file:663603-70-1.mol

Synonyms:663603-70-1;3-(METHYLAMINO)-1-(THIOPHEN-2-YL)PROP-2-EN-1-ONE;DTXSID00697651

Suppliers and Price of 3-(Methylamino)-1-(thiophen-2-YL)prop-2-EN-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-(Methylamino)-1-(thiophen-2-YL)prop-2-EN-1-one

Chemical Property:

PSA：57.34000
LogP:2.05480
XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:167.04048508
Heavy Atom Count:11
Complexity:168

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNC=CC(=O)C1=CC=CS1

Technology Process of 3-(Methylamino)-1-(thiophen-2-YL)prop-2-EN-1-one

There total 5 articles about 3-(Methylamino)-1-(thiophen-2-YL)prop-2-EN-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.8%

: 593-51-1
methylamine hydrochloride

: 130371-57-2
βeta;-oxo-βeta;-(2-thienyl)propanal sodium salt

: 663603-70-1
(Z)-3-(methylamino)-1-(thiophen-2-yl)prop-2-en-1-one

Guidance literature:: methylamine hydrochloride; βeta;-oxo-βeta;-(2-thienyl)propanal sodium salt; In methanol; water; at 25 - 30 ℃; for 5.33333h;

With sodium hydroxide; In water;

Reference yield: 74.8%

: 593-51-1
methylamine hydrochloride

: β-oxo-β-(2-thienyl)propanal sodium salt

: 663603-70-1
(Z)-3-(methylamino)-1-(thiophen-2-yl)prop-2-en-1-one

Guidance literature:: methylamine hydrochloride; β-oxo-β-(2-thienyl)propanal sodium salt; In methanol; water; at 25 - 30 ℃; for 5.3h;

With sodium hydroxide; In tert-butyl methyl ether; water;

In tert-butyl methyl ether; Product distribution / selectivity; crystallization; Seeding of (Z)-N-monomethyl-3-oxo-(2-thienyl)propenamine;