Dodecanoic acid, 2-[[(phenylmethoxy)carbonyl]amino]-, 4-nitrophenyl ester

Base Information

Chemical Name:Dodecanoic acid, 2-[[(phenylmethoxy)carbonyl]amino]-, 4-nitrophenyl ester
CAS No.:66398-13-8
Molecular Formula:C26H34N2O6
Molecular Weight:470.566
Hs Code.:

Synonyms:

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Chemical Property of Dodecanoic acid, 2-[[(phenylmethoxy)carbonyl]amino]-, 4-nitrophenyl ester

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Technology Process of Dodecanoic acid, 2-[[(phenylmethoxy)carbonyl]amino]-, 4-nitrophenyl ester

There total 3 articles about Dodecanoic acid, 2-[[(phenylmethoxy)carbonyl]amino]-, 4-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 66398-12-7
(+/-)-(benzyloxycarbonyl)-α-aminododecanoic acid

: 66398-13-8
(+/-)-p-nitrophenyl N-(benzyloxycarbonyl)-α-aminododecanoic acid

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; 1.) 0 deg C, 2 h, 2.) room temperature, 44 h;
DOI:10.1021/jm00398a027

Reference yield:

: 35237-37-7
2-amino-dodecanoic acid

: 66398-13-8
(+/-)-p-nitrophenyl N-(benzyloxycarbonyl)-α-aminododecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 46.2 percent / aq. NaOH / 1 h / 10 °C

2: 63 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 1.) 0 deg C, 2 h, 2.) room temperature, 44 h

With sodium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/jm00398a027

Reference yield:

: 111-56-8,201417-52-9
2-bromododecanoic acid

: 66398-13-8
(+/-)-p-nitrophenyl N-(benzyloxycarbonyl)-α-aminododecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / ammonium hydroxide / 168 h / Ambient temperature

2: 46.2 percent / aq. NaOH / 1 h / 10 °C

3: 63 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 1.) 0 deg C, 2 h, 2.) room temperature, 44 h

With ammonium hydroxide; sodium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/jm00398a027