1,4-Dioxaspiro[4.4]nonane-6-carbaldehyde

Base Information

Chemical Name:1,4-Dioxaspiro[4.4]nonane-6-carbaldehyde
CAS No.:66522-88-1
Molecular Formula:C₈H₁₂O₃
Molecular Weight:156.181
Hs Code.:2932999099
DSSTox Substance ID:DTXSID30561270

Synonyms:66522-88-1;1,4-dioxaspiro[4.4]nonane-6-carbaldehyde;DTXSID30561270

Suppliers and Price of 1,4-Dioxaspiro[4.4]nonane-6-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,4-Dioxaspiro[4.4]nonane-6-carbaldehyde

Chemical Property:

PSA：35.53000
LogP:0.72850
XLogP3:0
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:156.078644241
Heavy Atom Count:11
Complexity:161

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(C2(C1)OCCO2)C=O

Technology Process of 1,4-Dioxaspiro[4.4]nonane-6-carbaldehyde

There total 2 articles about 1,4-Dioxaspiro[4.4]nonane-6-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23153-74-4
(1,4-dioxa-spiro[4.4]non-6-yl)-methanol

: 66522-88-1
6-Formyl-1,4-dioxaspiro<4.4>nonane

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81545-3

Reference yield:

: 23153-73-3
ethyl 1,4-dioxaspiro[4,4]nonane-6-carboxylate

: 66522-88-1
6-Formyl-1,4-dioxaspiro<4.4>nonane

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / lithium aluminum hydride / diethyl ether / 1 h

2: PCC, AcONa / CH₂Cl₂ / 3 h / Ambient temperature

With lithium aluminium tetrahydride; sodium acetate; pyridinium chlorochromate; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)81545-3

Reference yield:

: 66522-88-1
6-Formyl-1,4-dioxaspiro<4.4>nonane

: 131923-99-4
(E)-6-Phenyl-hex-5-enoic acid 2-hydroxy-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 0.5 h / 0 °C

2: 75 percent / boron trifluoride etherate / CH₂Cl₂ / 14 h

With boron trifluoride diethyl etherate; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)81545-3