Benzene, 1-(3-butenyl)-2-ethenyl-

Base Information

Chemical Name:Benzene, 1-(3-butenyl)-2-ethenyl-
CAS No.:66657-91-8
Molecular Formula:C12H14
Molecular Weight:158.243
Hs Code.:2902909090
DSSTox Substance ID:DTXSID50454559
Nikkaji Number:J2.045.371K

Synonyms:66657-91-8;Benzene, 1-(3-butenyl)-2-ethenyl-;2-(3-Butenyl)styrene;4-(vinylphenyl)-1-butene;DTXSID50454559;AKOS006289104;1-(BUT-3-EN-1-YL)-2-ETHENYLBENZENE;N-HEPTYL4-(4-ETHOXYPHENOXYCARBONYL)PHENYLCARBONATE

Suppliers and Price of Benzene, 1-(3-butenyl)-2-ethenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-BUT-3-ENYL-2-VINYL-BENZENE 95.00%
5MG
$ 497.57

Total 7 raw suppliers

Chemical Property of Benzene, 1-(3-butenyl)-2-ethenyl-

Chemical Property:

PSA：0.00000
LogP:3.44820
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:158.109550447
Heavy Atom Count:12
Complexity:146

Purity/Quality:

99% ^*data from raw suppliers

1-BUT-3-ENYL-2-VINYL-BENZENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCCC1=CC=CC=C1C=C

Technology Process of Benzene, 1-(3-butenyl)-2-ethenyl-

There total 3 articles about Benzene, 1-(3-butenyl)-2-ethenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 106-95-6
allyl bromide

: 31955-56-3
1-[(benzyloxy)methyl]-2-vinylbenzene

: 66657-91-8
1-(3-butenyl)-2-vinylbenzene

Guidance literature:: 1-[(benzyloxy)methyl]-2-vinylbenzene; With n-butyllithium; zirconocene dichloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;

allyl bromide; With copper(l) chloride; In tetrahydrofuran; hexane; for 5h; Heating;
DOI:10.1021/jo048860b

Reference yield:

: 35106-82-2
2-vinylbenzylalcohol

: 66657-91-8
1-(3-butenyl)-2-vinylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / NaH / tetrahydrofuran / 0 - 20 °C

2.1: Cp₂ZrCl₂; n-BuLi / tetrahydrofuran; hexane / -78 - 20 °C

2.2: 88 percent / CuCl / tetrahydrofuran; hexane / 5 h / Heating

With n-butyllithium; zirconocene dichloride; sodium hydride; In tetrahydrofuran; hexane;
DOI:10.1021/jo048860b