Ethanone, 2-bromo-1-(3,4-dimethoxyphenyl)-2-phenyl-

Base Information

Chemical Name:Ethanone, 2-bromo-1-(3,4-dimethoxyphenyl)-2-phenyl-
CAS No.:66659-96-9
Molecular Formula:C16H15BrO3
Molecular Weight:335.197
Hs Code.:
DSSTox Substance ID:DTXSID70456378

Synonyms:Ethanone, 2-bromo-1-(3,4-dimethoxyphenyl)-2-phenyl-;66659-96-9;SCHEMBL11376411;DTXSID70456378

Suppliers and Price of Ethanone, 2-bromo-1-(3,4-dimethoxyphenyl)-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethanone, 2-bromo-1-(3,4-dimethoxyphenyl)-2-phenyl-

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:334.02046
Heavy Atom Count:20
Complexity:315

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C(=O)C(C2=CC=CC=C2)Br)OC

Technology Process of Ethanone, 2-bromo-1-(3,4-dimethoxyphenyl)-2-phenyl-

There total 3 articles about Ethanone, 2-bromo-1-(3,4-dimethoxyphenyl)-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 3141-93-3
4',5'-dimethoxydeoxybenzoin

: 66659-96-9
2-bromo-1-(3,4-dimethoxyphenyl)-2-phenylethanone

Guidance literature:: With bromine; In chloroform; for 3h; Heating;
DOI:10.1002/1099-0690(200207)2002:13<2126::AID-EJOC2126>3.0.CO;2-A

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 66659-96-9
2-bromo-1-(3,4-dimethoxyphenyl)-2-phenylethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 92.9 percent / AlCl₃ / 0.67 h / 20 °C

2: 47.3 percent / benzyltrimethyl-ammonium tribromide / CH₂Cl₂; methanol / 5 h / Heating

With aluminium trichloride; benzyltrimethylammonium tribromide; In methanol; dichloromethane; 1: Friedel-Crafts reaction;
DOI:10.3987/com-06-10853

Reference yield:

: 103-80-0
phenylacetyl chloride

: 66659-96-9
2-bromo-1-(3,4-dimethoxyphenyl)-2-phenylethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 92.9 percent / AlCl₃ / 0.67 h / 20 °C

2: 47.3 percent / benzyltrimethyl-ammonium tribromide / CH₂Cl₂; methanol / 5 h / Heating

With aluminium trichloride; benzyltrimethylammonium tribromide; In methanol; dichloromethane; 1: Friedel-Crafts reaction;
DOI:10.3987/com-06-10853