1-METHYL-2,3,4,9-TETRAHYDRO-1H-BETA-CARBOLINEHYDROCHLORIDE

Base Information

• Chemical Name: 1-METHYL-2,3,4,9-TETRAHYDRO-1H-BETA-CARBOLINEHYDROCHLORIDE
• CAS No.: 6678-82-6
• Molecular Formula: C12H14N2.ClH
• Molecular Weight: 222.718
• Mol file: 6678-82-6.mol

Synonyms:1-methyl-2,3,4,9-tetrahydro-1H-β-carboline, hydrochloride;1-Methyl-2,3,4,9-tetrahydro-1H-β-carbolin, Hydrochlorid;

Chemical Property of 1-METHYL-2,3,4,9-TETRAHYDRO-1H-BETA-CARBOLINEHYDROCHLORIDE

Chemical Property:

• Melting Point: 267℃
• PSA: 27.82000
• LogP: 3.50540

Purity/Quality:

98%min ^*data from raw suppliers

DL-EleagninHydrochloride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-METHYL-2,3,4,9-TETRAHYDRO-1H-BETA-CARBOLINEHYDROCHLORIDE

There total 2 articles about 1-METHYL-2,3,4,9-TETRAHYDRO-1H-BETA-CARBOLINEHYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

tryptamine (61-54-1) + acetaldehyde (75-07-0,9002-91-9) → (+/-)-Calligonine hydrochloride (6678-82-6)

Guidance literature:

With pyridine; chloro-trimethyl-silane; at 100 ℃; for 4h; Inert atmosphere;

DOI:10.1007/s00706-012-0804-7

Reference yield:

tryptamine hydochloride (343-94-2) + acetaldehyde (75-07-0,9002-91-9) → (+/-)-Calligonine hydrochloride (6678-82-6)

Guidance literature:

DOI:10.1021/cs400724g

Reference yield: 92.0%

(+/-)-Calligonine hydrochloride (6678-82-6) → harmane (486-84-0)

Guidance literature:

With 5 mol% Pd/C; lithium carbonate; In ethanol; at 150 ℃; for 0.1h; Sealed tube; Microwave irradiation;

DOI:10.1002/ejoc.201301580

upstream raw materials:

tryptamine

acetaldehyde

tryptamine hydochloride

Downstream raw materials:

(R)-1-methyl-1,2,3,4-tetrahydro-9H-pyrido[3,4-b]indole

harmane

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