1-(Chloromethyl)-2-methoxynaphthalene

Base Information

Chemical Name:1-(Chloromethyl)-2-methoxynaphthalene
CAS No.:67367-39-9
Molecular Formula:C12H11ClO
Molecular Weight:206.672
Hs Code.:2909309090
DSSTox Substance ID:DTXSID40538110
Nikkaji Number:J3.043.534F
Wikidata:Q82413335

Synonyms:1-(chloromethyl)-2-methoxynaphthalene;67367-39-9;Naphthalene, 1-(chloromethyl)-2-methoxy-;SCHEMBL4698919;DTXSID40538110;CGSYKRJQLUCLOR-UHFFFAOYSA-N;1-chloromethyl-2-methoxy-naphthalene;AKOS009476335;1-(chloromethyl)-2-naphthyl methyl ether;EN300-1981454;A916792;AB-131/42300712;F1911-3817

Suppliers and Price of 1-(Chloromethyl)-2-methoxynaphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-(Chloromethyl)-2-methoxynaphthalene
50mg
$ 130.00

Matrix Scientific
1-(Chloromethyl)-2-methoxynaphthalene 97%
1g
$ 398.00

Crysdot
1-(Chloromethyl)-2-methoxynaphthalene 95+%
1g
$ 420.00

Chemenu
1-(Chloromethyl)-2-methoxynaphthalene 95%
1g
$ 396.00

Atlantic Research Chemicals
1-(Chloromethyl)-2-methoxynaphthalene 95%
1gm:
$ 371.13

American Custom Chemicals Corporation
1-(CHLOROMETHYL)-2-METHOXYNAPHTHALENE 95.00%
5MG
$ 504.66

Alichem
1-(Chloromethyl)-2-methoxynaphthalene
1g
$ 1769.25

Alichem
1-(Chloromethyl)-2-methoxynaphthalene
500mg
$ 970.20

Alichem
1-(Chloromethyl)-2-methoxynaphthalene
250mg
$ 659.60

Total 5 raw suppliers

Chemical Property of 1-(Chloromethyl)-2-methoxynaphthalene

Chemical Property:

Melting Point:120 °C (decomp)
Boiling Point:328.2±17.0 °C(Predicted)
PSA：9.23000
Density:1.179±0.06 g/cm3(Predicted)
LogP:3.58720
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:206.0498427
Heavy Atom Count:14
Complexity:183

Purity/Quality:

97% ^*data from raw suppliers

1-(Chloromethyl)-2-methoxynaphthalene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C2=CC=CC=C2C=C1)CCl

Technology Process of 1-(Chloromethyl)-2-methoxynaphthalene

There total 5 articles about 1-(Chloromethyl)-2-methoxynaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 40696-22-8
(2-methoxy-naphthalene-1-yl)-methanol

: 67367-39-9
1-chloromethyl-2-methoxynaphthalene

Guidance literature:: With thionyl chloride; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/ja300164d

Reference yield:

: 5392-12-1
2-methoxy-1-naphthaldehyde

: 67367-39-9
1-chloromethyl-2-methoxynaphthalene

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water;

Reference yield:

: 93-04-9
2-Methoxynaphthalene

: 67367-39-9
1-chloromethyl-2-methoxynaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 1,2-dichloro-ethane / 8 h / 0 °C / Inert atmosphere; Reflux

1.2: Inert atmosphere; Cooling with ice

2.1: sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: thionyl chloride / dichloromethane / 0 °C / Inert atmosphere

With sodium tetrahydroborate; thionyl chloride; trichlorophosphate; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ja300164d