1-(2,4-Dinitrophenyl)-2-(4-nitrophenyl)hydrazine

Base Information

• Chemical Name: 1-(2,4-Dinitrophenyl)-2-(4-nitrophenyl)hydrazine
• CAS No.: 67449-74-5
• Molecular Formula: C12H9N5O6
• Molecular Weight: 319.233
• DSSTox Substance ID: DTXSID30397192
• Wikidata: Q82198321
• Mol file: 67449-74-5.mol

Synonyms:1-(2,4-dinitrophenyl)-2-(4-nitrophenyl)hydrazine;67449-74-5;DTXSID30397192;STK046099;AKOS000489831

Chemical Property of 1-(2,4-Dinitrophenyl)-2-(4-nitrophenyl)hydrazine

Chemical Property:

• XLogP3: 3.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 3
• Exact Mass: 319.05528302
• Heavy Atom Count: 23
• Complexity: 450

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC=C1NNC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 1-(2,4-Dinitrophenyl)-2-(4-nitrophenyl)hydrazine

There total 2 articles about 1-(2,4-Dinitrophenyl)-2-(4-nitrophenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chlorobenzonitrile (100-00-5) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → N-(2,4-dinitro-phenyl)-N'-(4-nitro-phenyl)-hydrazine (67449-74-5)

Guidance literature:

With potassium nitrate modified alumina solid base; In dichloromethane; at 20 - 40 ℃; for 1.5h; Sonication; Green chemistry;

Reference yield:

4-nitrophenylhydrazone (100-16-3) + 1-chloro-2,4-dinitro-benzene (97-00-7) → N-(2,4-dinitro-phenyl)-N'-(4-nitro-phenyl)-hydrazine (67449-74-5)

Guidance literature:

at 100 - 105 ℃;

Reference yield:

N-(2,4-dinitro-phenyl)-N'-(4-nitro-phenyl)-hydrazine (67449-74-5) → (2,4-dinitrophenylazo)-4-nitrobenzene

Guidance literature:

With dihydrogen peroxide; In dichloromethane; at 20 ℃; for 4h; Green chemistry;

upstream raw materials:

4-nitrophenylhydrazone

1-chloro-2,4-dinitro-benzene

4-chlorobenzonitrile

(2,4-dinitro-phenyl)-hydrazine

Downstream raw materials:

(2,4-dinitro-phenyl)-(4-nitro-phenyl)-diazene

Refernces