n-(2-Methylpropyl)-n-nitrosoacetamide

Base Information

• Chemical Name: n-(2-Methylpropyl)-n-nitrosoacetamide
• CAS No.: 15289-94-8
• Molecular Formula: C6H12 N2 O2
• Molecular Weight: 144.173
• NSC Number: 95271
• DSSTox Substance ID: DTXSID20934631
• Wikidata: Q82910542
• Mol file: 15289-94-8.mol

Synonyms:15289-94-8;n-(2-methylpropyl)-n-nitrosoacetamide;NSC95271;DTXSID20934631;NSC-95271

Chemical Property of n-(2-Methylpropyl)-n-nitrosoacetamide

Chemical Property:

• Vapor Pressure: 1.16mmHg at 25°C
• Boiling Point: 175.2°C at 760 mmHg
• Flash Point: 59.8°C
• Density: 1.05g/cm³
• XLogP3: 0.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 144.089877630
• Heavy Atom Count: 10
• Complexity: 134

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)CN(C(=O)C)N=O

Technology Process of n-(2-Methylpropyl)-n-nitrosoacetamide

There total 1 articles about n-(2-Methylpropyl)-n-nitrosoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-isobutylacetamide (1540-94-9) → N-isobutyl-N-nitroso-acetamide (15289-94-8)

Guidance literature:

With sodium nitrite;

DOI:10.1021/ja01627a064

Reference yield:

tetrachloromethane (56-23-5) + N-isobutyl-N-nitroso-acetamide (15289-94-8) → acetic acid tert-butyl ester (540-88-5) + sec-Butyl acetate (105-46-4) + 2-methylpropyl acetate (110-19-0)

Guidance literature:

at 77 ℃;

DOI:10.1021/ja01627a064

upstream raw materials:

N-isobutylacetamide

Downstream raw materials:

acetic acid tert-butyl ester

sec-Butyl acetate

2-methylpropyl acetate