Cyclohexanone, 2-acetyl-2-(2-propenyl)-

Base Information

Chemical Name:Cyclohexanone, 2-acetyl-2-(2-propenyl)-
CAS No.:67679-11-2
Molecular Formula:C11H16O2
Molecular Weight:180.247
Hs Code.:
DSSTox Substance ID:DTXSID20477957
Nikkaji Number:J1.949.642B

Synonyms:67679-11-2;Cyclohexanone, 2-acetyl-2-(2-propenyl)-;DTXSID20477957

Suppliers and Price of Cyclohexanone, 2-acetyl-2-(2-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Cyclohexanone, 2-acetyl-2-(2-propenyl)-

Chemical Property:

PSA：34.14000
LogP:2.28100
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:180.115029749
Heavy Atom Count:13
Complexity:243

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1(CCCCC1=O)CC=C

Technology Process of Cyclohexanone, 2-acetyl-2-(2-propenyl)-

There total 4 articles about Cyclohexanone, 2-acetyl-2-(2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 874-23-7,125117-37-5
2-acetylcyclohexanone

: 107-18-6
allyl alcohol

: 67679-11-2
2-acetyl-2-(2-propenyl)cyclohexanone

Guidance literature:: With triethyl borane; potassium hexamethylsilazane; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; In tetrahydrofuran; at 50 ℃; for 2h;
DOI:10.1016/S0040-4020(03)01234-1

Reference yield: 83.0%

: 591-87-7
Allyl acetate

: 874-23-7,125117-37-5
2-acetylcyclohexanone

: 67679-11-2
2-acetyl-2-(2-propenyl)cyclohexanone

Guidance literature:: With L-Valine methyl ester; 4-[bis(2-diphenylphosphanyl)ethyl]amino-4-oxobutanoic acid; sodium hydride; bis(η3-allyl-μ-chloropalladium(II)); In tetrahydrofuran; at -30 ℃; Product distribution; var. of reagent, catalyst, temp.; asymmetric induction;
DOI:10.1039/c39820001162

Reference yield:

: 874-23-7,125117-37-5
2-acetylcyclohexanone

: 106-95-6
allyl bromide

: 94-66-6
2-allylcyclohexan-1-one

: 67679-11-2
2-acetyl-2-(2-propenyl)cyclohexanone

Guidance literature:: With sodium hydroxide; In water; for 2h; Title compound not separated from byproducts; Ambient temperature; pH 10.8;
DOI:10.1021/ja00034a040