2-Bromo-2-phenyl-1-(3-pyridyl)ethanone hydrobromide

Base Information

Chemical Name:2-Bromo-2-phenyl-1-(3-pyridyl)ethanone hydrobromide
CAS No.:67947-67-5
Molecular Formula:C13H10BrNO.BrH
Molecular Weight:357.044
Hs Code.:
DSSTox Substance ID:DTXSID50541539

Synonyms:67947-67-5;2-bromo-2-phenyl-1-(3-pyridyl)ethanone hydrobromide;SCHEMBL6546257;DTXSID50541539;FDZYXELONZKFES-UHFFFAOYSA-N;3-pyridyl alpha-bromobenzyl ketone hydrobromide;2-Bromo-2-phenyl-1-(3-pyridyl)-ethanone hydrobromide;2-Bromo-2-phenyl-1-(pyridin-3-yl)ethan-1-one--hydrogen bromide (1/1)

Suppliers and Price of 2-Bromo-2-phenyl-1-(3-pyridyl)ethanone hydrobromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-Bromo-2-phenyl-1-(3-pyridyl)ethanone hydrobromide

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:356.91869
Heavy Atom Count:17
Complexity:238

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(C(=O)C2=CN=CC=C2)Br.Br

Technology Process of 2-Bromo-2-phenyl-1-(3-pyridyl)ethanone hydrobromide

There total 6 articles about 2-Bromo-2-phenyl-1-(3-pyridyl)ethanone hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 14627-92-0
2-phenyl-1-(pyridin-3-yl)ethanone

: 67947-67-5
2-bromo-2-phenyl-1-(pyridin-3-yl)-ethanone hydrobromide

Guidance literature:: With bromine; In acetic acid; for 2h; Ambient temperature;

Reference yield:

: 5-phenyl-4-(pyridin-3-yl)-thiazoline-2-thione

: 84263-30-9
2-phenyl-1-[3]pyridyl-ethanone; hydrobromide

: 74-88-4
methyl iodide

: 67947-67-5
2-bromo-2-phenyl-1-(pyridin-3-yl)-ethanone hydrobromide

Guidance literature:: With bromine; In N,N,N,N,N,N-hexamethylphosphoric triamide; ice-water; diethyl ether; water; acetic acid; ethyl acetate; mineral oil;

Reference yield:

: 100-39-0
benzyl bromide

: 67947-67-5
2-bromo-2-phenyl-1-(pyridin-3-yl)-ethanone hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: diisopropylamin, n-butyllithium (15 percent), / hexane; tetrahydrofuran / 1 h / -78 °C

2: tetrabutylammoniumfluorid-hydrat / hexane; tetrahydrofuran; CH₂Cl₂ / Ambient temperature; stirring overnight

3: 82 percent / brom / acetic acid / 2 h / Ambient temperature

With n-butyllithium; tetrabutyl ammonium fluoride; bromine; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; acetic acid;