2-Iodo-N,N-dimethyl-4-nitrobenzenamine

Base Information

Chemical Name:2-Iodo-N,N-dimethyl-4-nitrobenzenamine
CAS No.:681259-73-4
Molecular Formula:C8H9IN2O2
Molecular Weight:292.076
Hs Code.:
DSSTox Substance ID:DTXSID901282820
Nikkaji Number:J2.278.296G

Synonyms:681259-73-4;DTXSID901282820;2-Iodo-N,N-dimethyl-4-nitrobenzenamine

Suppliers and Price of 2-Iodo-N,N-dimethyl-4-nitrobenzenamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Iodo-N,N-dimethyl-4-nitrobenzenamine

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:291.97088
Heavy Atom Count:13
Complexity:193

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C)C1=C(C=C(C=C1)[N+](=O)[O-])I

Technology Process of 2-Iodo-N,N-dimethyl-4-nitrobenzenamine

There total 2 articles about 2-Iodo-N,N-dimethyl-4-nitrobenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 100-23-2
N,N-Dimethyl-4-nitroaniline

: 681259-73-4
N,N-dimethyl-2-iodo-4-nitroaniline

Guidance literature:: With sodium periodate; sulfuric acid; dihydrogen peroxide; In ethanol; water; at 50 ℃; for 0.5h;

Reference yield: 75.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 6293-83-0
2-iodo-4-nitrophenylamine

: 681259-73-4
N,N-dimethyl-2-iodo-4-nitroaniline

Guidance literature:: formaldehyd; 2-iodo-4-nitrophenylamine; In 2,2,2-trifluoroethanol; for 1h; Reflux;

With sodium tetrahydroborate; In 2,2,2-trifluoroethanol; for 8h; Reflux;
DOI:10.1021/ol401303f

Reference yield: 100.0%

: 931-49-7
1-ethenylcyclohexene

: 681259-73-4
N,N-dimethyl-2-iodo-4-nitroaniline

: N,N-dimethyl-2-(cyclohex-1-enylethynyl)-4-nitroaniline

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; at 20 ℃; for 5h;
DOI:10.1021/jo051549p