N,N-Diethyl 4-bromo-2-chlorobenzamide

Base Information

Chemical Name:N,N-Diethyl 4-bromo-2-chlorobenzamide
CAS No.:682778-17-2
Molecular Formula:C11H13BrClNO
Molecular Weight:290.587
Hs Code.:2924299090
DSSTox Substance ID:DTXSID70583037
Wikidata:Q82474548
Mol file:682778-17-2.mol

Synonyms:N,N-Diethyl 4-bromo-2-chlorobenzamide;682778-17-2;4-Bromo-2-chloro-N,N-diethylbenzamide;SCHEMBL3552169;DTXSID70583037;IFMVHORCFRIXQD-UHFFFAOYSA-N;MFCD20046464;N,N-Diethyl4-bromo-2-chlorobenzamide;AKOS010133924;N,N-diethyl-4-bromo-2-chlorobenzamide;BS-24553;CS-0194499;E91912

Suppliers and Price of N,N-Diethyl 4-bromo-2-chlorobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N,N-Diethyl4-bromo-2-chlorobenzamide
1g
$ 115.00

Crysdot
N,N-Diethyl4-bromo-2-chlorobenzamide 95+%
10g
$ 395.00

AOBChem
N,N-dimethyl4-bromo-2-chlorobenzamide 97%
25g
$ 762.00

Total 3 raw suppliers

Chemical Property of N,N-Diethyl 4-bromo-2-chlorobenzamide

Chemical Property:

PSA：20.31000
LogP:3.58450
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:288.98690
Heavy Atom Count:15
Complexity:221

Purity/Quality:

99% ^*data from raw suppliers

N,N-Diethyl4-bromo-2-chlorobenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=C(C=C(C=C1)Br)Cl

Technology Process of N,N-Diethyl 4-bromo-2-chlorobenzamide

There total 3 articles about N,N-Diethyl 4-bromo-2-chlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 21900-55-0
4-bromo-2-chlorobenzoyl chloride

: 109-89-7
diethylamine

: 682778-17-2
N,N-diethyl-4-bromo-2-chlorobenzamide

Guidance literature:: In dichloromethane; for 0.25h;
DOI:10.1021/jm0612968

Reference yield:

: 59748-90-2
4-Bromo-2-chloro-benzoic Acid

: 682778-17-2
N,N-diethyl-4-bromo-2-chlorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / DMF / CH₂Cl₂ / 4 h

2: 100 percent / CH₂Cl₂ / 0.25 h

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/jm0612968