Sulfamic acid, dimethyl-, 7-[(4-fluorophenyl)methyl]-7,8-dihydro-6,8-dioxo-9-[[tris(1-methylethyl)sil yl]oxy]-6H-pyrrolo[3,4-g]quinolin-5-yl ester

Base Information

Chemical Name:Sulfamic acid, dimethyl-, 7-[(4-fluorophenyl)methyl]-7,8-dihydro-6,8-dioxo-9-[[tris(1-methylethyl)sil yl]oxy]-6H-pyrrolo[3,4-g]quinolin-5-yl ester
CAS No.:684285-24-3
Molecular Formula:C29H36FN3O6SSi
Molecular Weight:601.771
Hs Code.:

Sulfamic acid, dimethyl-,
7-[(4-fluorophenyl)methyl]-7,8-dihydro-6,8-dioxo-9-[[tris(1-methylethyl)sil
yl]oxy]-6H-pyrrolo[3,4-g]quinolin-5-yl ester

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Chemical Property of Sulfamic acid, dimethyl-, 7-[(4-fluorophenyl)methyl]-7,8-dihydro-6,8-dioxo-9-[[tris(1-methylethyl)sil yl]oxy]-6H-pyrrolo[3,4-g]quinolin-5-yl ester

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Technology Process of Sulfamic acid, dimethyl-, 7-[(4-fluorophenyl)methyl]-7,8-dihydro-6,8-dioxo-9-[[tris(1-methylethyl)sil yl]oxy]-6H-pyrrolo[3,4-g]quinolin-5-yl ester

There total 3 articles about Sulfamic acid, dimethyl-, 7-[(4-fluorophenyl)methyl]-7,8-dihydro-6,8-dioxo-9-[[tris(1-methylethyl)sil yl]oxy]-6H-pyrrolo[3,4-g]quinolin-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 684284-38-6
7-(4-fluorobenzyl)-5-hydroxy-9-triisopropylsilanyloxypyrrolo[3,4-g]quinoline-6,8-dione

: 13360-57-1
dimethylamino sulfonyl chloride

: 684285-24-3
dimethylsulfamic acid 7-(4-fluoro-benzyl)-6,8-dioxo-9-triisopropylsilanyloxy-7,8-dihydro-6H-pyrrolo[3,4-g]quinolin-5-yl ester

Guidance literature:: With dmap; TEA; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2006.05.008

Reference yield:

: 684284-29-5
7-(4-fluoro-benzyl)-5,9-dihydroxy-pyrrolo[3,4-g]quinoline-6,8-dione

: 684285-24-3
dimethylsulfamic acid 7-(4-fluoro-benzyl)-6,8-dioxo-9-triisopropylsilanyloxy-7,8-dihydro-6H-pyrrolo[3,4-g]quinolin-5-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 36 h

2: 75 percent / DMAP; TEA / CH₂Cl₂ / 2 h / 20 °C

With 1H-imidazole; dmap; TEA; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.05.008

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 684285-24-3
dimethylsulfamic acid 7-(4-fluoro-benzyl)-6,8-dioxo-9-triisopropylsilanyloxy-7,8-dihydro-6H-pyrrolo[3,4-g]quinolin-5-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 36 h

2: 75 percent / DMAP; TEA / CH₂Cl₂ / 2 h / 20 °C

With 1H-imidazole; dmap; TEA; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.05.008