6-Phenoxypicolinaldehyde

Base Information

Chemical Name:6-Phenoxypicolinaldehyde
CAS No.:68523-22-8
Molecular Formula:C12H9NO2
Molecular Weight:199.209
Hs Code.:
DSSTox Substance ID:DTXSID10513530
Wikidata:Q82373390

Synonyms:6-Phenoxypicolinaldehyde;68523-22-8;6-phenoxypyridine-2-carbaldehyde;107054-96-6;2-Pyridinecarboxaldehyde, 6-phenoxy-;2-formyl-6-phenoxypyridine;6-(phenoxy)-picolinaldehyde;2-formyl-6-phenoxy-pyridine;SCHEMBL9540409;DTXSID10513530;YZFJCORZVYKNLY-UHFFFAOYSA-N;6-phenoxy-2-pyridinecarboxaldehyde;6-Phenoxypyridine-2-carboxaldehyde;AKOS002263313;SB53962

Suppliers and Price of 6-Phenoxypicolinaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 6-Phenoxypicolinaldehyde

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:199.063328530
Heavy Atom Count:15
Complexity:202

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)OC2=CC=CC(=N2)C=O

Technology Process of 6-Phenoxypicolinaldehyde

There total 7 articles about 6-Phenoxypicolinaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.6%

: 83247-00-1
2-bromo-6-phenoxypyridine

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 4783-68-0
2-phenoxypyridine

: 68523-22-8
6-phenoxy-pyridin-2-ylcarboxaldehyde

Guidance literature:: With ethylmagnesium bromide; In tetrahydrofuran; at 20 ℃; for 3h; Product distribution; variation of reagent;
DOI:10.1246/cl.1985.1803

Reference yield: 32.0%

: C₁₅H₁₅NO₃

: 68523-22-8
6-phenoxy-pyridin-2-ylcarboxaldehyde

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water;
DOI:10.1016/j.ejmech.2021.113784

Reference yield:

: 83247-00-1
2-bromo-6-phenoxypyridine

: 122-51-0
orthoformic acid triethyl ester

: 4783-68-0
2-phenoxypyridine

: 68523-22-8
6-phenoxy-pyridin-2-ylcarboxaldehyde

Guidance literature:: With magnesium; methyl iodide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, 40-45 deg C, 1.5 h, 2.) 10 deg C, 20 deg C, 3 h, 40 deg C, 0.5 h;
DOI:10.1246/cl.1985.1803