Tetrahydro-4-methyl-2-phenyl-2H-pyran

Base Information

Chemical Name:Tetrahydro-4-methyl-2-phenyl-2H-pyran
CAS No.:94201-73-7
Molecular Formula:C12H16 O
Molecular Weight:176.258
Hs Code.:2932999099
European Community (EC) Number:303-662-1
DSSTox Substance ID:DTXSID90869209
Nikkaji Number:J382.467E
Mol file:94201-73-7.mol

Synonyms:Tetrahydro-4-methyl-2-phenyl-2H-pyran;94201-73-7;4-methyl-2-phenyloxane;EINECS 303-662-1;4-methyl-2-phenyltetrahydro-2h-pyran;EC 303-662-1;2H-Pyran, tetrahydro-4-methyl-2-phenyl-;SCHEMBL1396587;DTXSID90869209;GDAVABNCFOTAOD-UHFFFAOYSA-N;tetrahydro - 4 - methyl - 2 - phenyl - 2H - pyran

Suppliers and Price of Tetrahydro-4-methyl-2-phenyl-2H-pyran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 11 raw suppliers

Chemical Property of Tetrahydro-4-methyl-2-phenyl-2H-pyran

Chemical Property:

Vapor Pressure:0.0152mmHg at 25°C
Boiling Point:265.3°Cat760mmHg
Flash Point:110.1°C
PSA：9.23000
Density:0.97g/cm³
LogP:3.17420
Water Solubility.:213mg/L at 20℃
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:176.120115130
Heavy Atom Count:13
Complexity:149

Purity/Quality:: 99.9% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCOC(C1)C2=CC=CC=C2

Technology Process of Tetrahydro-4-methyl-2-phenyl-2H-pyran

There total 5 articles about Tetrahydro-4-methyl-2-phenyl-2H-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3-methyl-1-phenylpentane-1,5-diol

: 94201-73-7,149713-23-5,149713-24-6
doremox

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

Reference yield: 75.0%

: 3-methyl-1-phenyl-4-penten-1-ol

: 94201-73-7,149713-23-5,149713-24-6
doremox

Guidance literature:: With trifluoroacetic acid;
DOI:10.1021/acscatal.0c00019

Reference yield:

: 98-86-2
acetophenone

: 94201-73-7,149713-23-5,149713-24-6
doremox

Guidance literature:: Multi-step reaction with 3 steps

1.1: bis(1,5-cyclooctadiene)nickel ⁽⁰⁾ / water / 2 h / 130 °C / Glovebox; Sealed tube

2.1: dimethylsulfide borane complex / tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 1 h / 0 °C

3.1: trifluorormethanesulfonic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; trifluorormethanesulfonic acid; dimethylsulfide borane complex; In tetrahydrofuran; dichloromethane; water;