Stannane, tributyl(2,4,6-trimethylphenyl)-

Base Information

• Chemical Name: Stannane, tributyl(2,4,6-trimethylphenyl)-
• CAS No.: 68971-91-5
• Molecular Formula: C21H38Sn
• Molecular Weight: 409.243
• DSSTox Substance ID: DTXSID60458927

Synonyms:Stannane, tributyl(2,4,6-trimethylphenyl)-;68971-91-5;DTXSID60458927;NTOFNMITMDFBSZ-UHFFFAOYSA-N;TRIBUTYL(2,4,6-TRIMETHYLPHENYL)STANNANE

Chemical Property of Stannane, tributyl(2,4,6-trimethylphenyl)-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 10
• Exact Mass: 410.199554
• Heavy Atom Count: 22
• Complexity: 252

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCCC[Sn](CCCC)(CCCC)C1=C(C=C(C=C1C)C)C

Technology Process of Stannane, tributyl(2,4,6-trimethylphenyl)-

There total 12 articles about Stannane, tributyl(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tributyltin chloride (1461-22-9) + 2-mesitylmagnesium bromide (2633-66-1) → tri-n-butyl(mesityl)stannane (68971-91-5)

Guidance literature:

In tetrahydrofuran; at -78 - 23 ℃;

Reference yield: 22.0%

1-fluoro-2,4,6-trimethylbenzene (392-69-8) + trimethylsilyltributyltin (17955-46-3) → tri-n-butyl(mesityl)stannane (68971-91-5)

Guidance literature:

With cesium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Irradiation; Schlenk technique; Sealed tube;

DOI:10.1021/jacs.1c00887

Reference yield:

tri-n-butyltin lithium (4226-01-1) + 2,4,6-trimethylphenyl bromide (576-83-0) → tri-n-butyl(mesityl)stannane (68971-91-5)

Guidance literature:

at 20 ℃;

upstream raw materials:

tributyltin chloride

2-mesitylmagnesium bromide

2,4,6-trimethylphenyl bromide

[Au(mesityl)(AsPh₃)]

Downstream raw materials:

1-(2,4,6-trimethylphenyl)naphthalene

1-fluoro-2,4,6-trimethylbenzene

2,4,6-Trimethylbenzophenon

[Au(mesityl)(AsPh₃)]

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