7-Pentadecyne, 9-methylene-

Base Information

Chemical Name:7-Pentadecyne, 9-methylene-
CAS No.:69520-29-2
Molecular Formula:C16H28
Molecular Weight:220.398
Hs Code.:
DSSTox Substance ID:DTXSID70473545
Nikkaji Number:J1.363.714H
Wikidata:Q82303014

Synonyms:9-methylene-pentadec-7-yne;7-Pentadecyne, 9-methylene-;2-hexyl-1-decen-3-yne;69520-29-2;7-methylenepentadec-8-yne;DTXSID70473545

Suppliers and Price of 7-Pentadecyne, 9-methylene-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 7-Pentadecyne, 9-methylene-

Chemical Property:

XLogP3:7.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:10
Exact Mass:220.219100893
Heavy Atom Count:16
Complexity:223

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCC#CC(=C)CCCCCC

Technology Process of 7-Pentadecyne, 9-methylene-

There total 5 articles about 7-Pentadecyne, 9-methylene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 629-05-0
n-octyne

: N,N,N'-trimethyl-N'-allylthiourea

: 201230-82-2
carbon monoxide

: 93161-32-1
hexadec-7-en-9-yne

: 1235569-12-6
C₁₂H₁₈O

: 69520-29-2
2-hexyl-1-decen-3-yne

: 10069-28-0
1,2,4-tri-n-hexylbenzene

: 29536-28-5
1,3,5-trihexylbenzene

Guidance literature:: dicobalt octacarbonyl; n-octyne; N,N,N'-trimethyl-N'-allylthiourea; With 1,1,3,3-tetramethyl-2-thiourea; In toluene; for 0.0833333h; Inert atmosphere;

carbon monoxide; In toluene; at 110 ℃; for 15h; under 2250.23 Torr; Autoclave;
DOI:10.1016/j.tetlet.2010.04.025

Reference yield:

: 629-05-0
n-octyne

: 3032-92-6
4-cyanophenylacetylene

: 69520-29-2
2-hexyl-1-decen-3-yne

: 4-(3-methylenenon-1-ynyl)benzonitrile

Guidance literature:: With C₉₂H₁₂₄Au₂Cl₂N₆O₈P₂; silver trifluoromethanesulfonate; In toluene; at 20 ℃; for 24h; Overall yield = 15 %;
DOI:10.1002/ejoc.201600362

Reference yield:

: 629-05-0
n-octyne

: 30309-80-9
di-o-tolylphosphine oxide

: C₂₂H₂₉OP

: 69520-29-2
2-hexyl-1-decen-3-yne

Guidance literature:: With tris(triphenylphosphine)rhodium(l) chloride; at 145 ℃; for 0.0833333h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.jorganchem.2010.08.024