4-Azidobutyrophenone

Base Information

Chemical Name:4-Azidobutyrophenone
CAS No.:69573-41-7
Molecular Formula:C10H11N3O
Molecular Weight:189.217
Hs Code.:
DSSTox Substance ID:DTXSID30446795
Nikkaji Number:J919.535A
Wikidata:Q82265520

Synonyms:4-Azidobutyrophenone;4-azido-1-phenylbutan-1-one;69573-41-7;gamma-azidobutyrophenone;SCHEMBL14583555;DTXSID30446795;ANHVCCDCYXVHNY-UHFFFAOYSA-N;AKOS019036948

Suppliers and Price of 4-Azidobutyrophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4-Azidobutyrophenone

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:189.090211983
Heavy Atom Count:14
Complexity:228

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)CCCN=[N+]=[N-]

Technology Process of 4-Azidobutyrophenone

There total 6 articles about 4-Azidobutyrophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 939-52-6
4-chloro-1-phenylbutan-1-one

: 69573-41-7
γ-azidobutyrophenone

Guidance literature:: With sodium azide; In dimethyl sulfoxide; at 55 ℃; for 60h;

Reference yield: 95.0%

: 24070-52-8
4-bromo-1-phenyl-1-butanone

: 69573-41-7
γ-azidobutyrophenone

Guidance literature:: With sodium azide; In dimethyl sulfoxide; for 0.133333h; Microwave irradiation;
DOI:10.1021/ol900754a

Reference yield: 85.0%

: 935-64-8
1-phenyl-1-cyclobutanol

: 69573-41-7
γ-azidobutyrophenone

Guidance literature:: With [2,2]bipyridinyl; 1-hydroxy-1,2-benzodioxol-3-(1H)-one; trimethylsilylazide; manganese(III) triacetate dihydrate; In acetonitrile; at 70 ℃; for 8h; Reagent/catalyst; Solvent; regiospecific reaction; Catalytic behavior; Inert atmosphere;
DOI:10.1002/anie.201506578