2-(3-Methylbut-2-en-1-yl)-2-phenyl-1,3-dioxolane

Base Information

Chemical Name:2-(3-Methylbut-2-en-1-yl)-2-phenyl-1,3-dioxolane
CAS No.:69803-72-1
Molecular Formula:C₁₄H₁₈O₂
Molecular Weight:218.296
Hs Code.:
DSSTox Substance ID:DTXSID10527910

Synonyms:69803-72-1;2-(3-Methylbut-2-en-1-yl)-2-phenyl-1,3-dioxolane;SCHEMBL3093084;DTXSID10527910

Suppliers and Price of 2-(3-Methylbut-2-en-1-yl)-2-phenyl-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-(3-Methylbut-2-en-1-yl)-2-phenyl-1,3-dioxolane

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:218.130679813
Heavy Atom Count:16
Complexity:242

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CCC1(OCCO1)C2=CC=CC=C2)C

Technology Process of 2-(3-Methylbut-2-en-1-yl)-2-phenyl-1,3-dioxolane

There total 3 articles about 2-(3-Methylbut-2-en-1-yl)-2-phenyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 69803-70-9
3-diphenylphosphinoyl-4-hydroxy-4-methyl-1-phenylpentan-1-one ethylene acetal

: 69803-72-1
5-methylyl-1-phenylpent-3-en-2-one ethylene acetal

: 69803-67-4
4-diphenylphosphinoylpentan-2-one ethylene acetal

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 20h; Ambient temperature;

Reference yield:

: 69803-60-7
(β-benzoylethyl)diphenylphosphine oxide

: 69803-72-1
5-methylyl-1-phenylpent-3-en-2-one ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / TsOH / benzene / Heating

2: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 5 min

3: 55 percent / NaH / tetrahydrofuran / 20 h / Ambient temperature

With n-butyllithium; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; benzene;

Reference yield:

: 69803-69-6
3-diphenylphosphinoyl-1-phenylpropan-1-one ethylene acetal

: 69803-72-1
5-methylyl-1-phenylpent-3-en-2-one ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 5 min

2: 55 percent / NaH / tetrahydrofuran / 20 h / Ambient temperature

With n-butyllithium; sodium hydride; In tetrahydrofuran;