Oxo(diphenyl)[2-(2-phenyl-1,3-dioxolan-2-yl)ethyl]-lambda~5~-phosphane

Base Information

Chemical Name:Oxo(diphenyl)[2-(2-phenyl-1,3-dioxolan-2-yl)ethyl]-lambda~5~-phosphane
CAS No.:69803-69-6
Molecular Formula:C23H23O3P
Molecular Weight:378.408
Hs Code.:
DSSTox Substance ID:DTXSID00527904
Wikidata:Q82397126

Synonyms:69803-69-6;DTXSID00527904;Oxo(diphenyl)[2-(2-phenyl-1,3-dioxolan-2-yl)ethyl]-lambda~5~-phosphane

Suppliers and Price of Oxo(diphenyl)[2-(2-phenyl-1,3-dioxolan-2-yl)ethyl]-lambda~5~-phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Oxo(diphenyl)[2-(2-phenyl-1,3-dioxolan-2-yl)ethyl]-lambda~5~-phosphane

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:378.13848159
Heavy Atom Count:27
Complexity:474

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1COC(O1)(CCP(=O)(C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of Oxo(diphenyl)[2-(2-phenyl-1,3-dioxolan-2-yl)ethyl]-lambda~5~-phosphane

There total 1 articles about Oxo(diphenyl)[2-(2-phenyl-1,3-dioxolan-2-yl)ethyl]-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 69803-60-7
(β-benzoylethyl)diphenylphosphine oxide

: 107-21-1
ethylene glycol

: 69803-69-6
3-diphenylphosphinoyl-1-phenylpropan-1-one ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;

Reference yield:

: 69803-69-6
3-diphenylphosphinoyl-1-phenylpropan-1-one ethylene acetal

: 69803-67-4
4-diphenylphosphinoylpentan-2-one ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 5 min

2: 24 percent / NaH / tetrahydrofuran / 20 h / Ambient temperature

With n-butyllithium; sodium hydride; In tetrahydrofuran;

Reference yield:

: 69803-69-6
3-diphenylphosphinoyl-1-phenylpropan-1-one ethylene acetal

: 69803-71-0
4-diphenylphosphinoyl-5-hydroxy-4-methyl-5-phenylpentan-2-one ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 5 min

2: 24 percent / NaH / tetrahydrofuran / 20 h / Ambient temperature

3: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 5 min, 2.) 10 min

With n-butyllithium; sodium hydride; In tetrahydrofuran;